5,5,5-三氟-4-氧戊酸乙酯合成路线 （共 6 条）
反应条件
boric acid T=170°C; 3 h; Heating;
参考文献
Ratier, Max; Pereyre, Michel; Davies, Alwyn G.; Sutcliffe, Roger
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , p. 1907 - 1916
反应条件
formic acid T=25°C; 12 h;
参考文献
Leyendecker, Joachim; Niewoehner, Ulrich; Steglich, Wolfgang
Tetrahedron Letters, 1983 , vol. 24, # 23 p. 2375 - 2378
反应条件
1: NaOEt 2: 62 percent / boric acid / 3 h / 170 °C / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1907 - 1916
反应条件
1: 95 percent / hydrogen / platinum oxide / diethyl ether / 760 Torr 3: 65 percent / potassium t-butoxide / dimethylsulfoxide View Scheme
参考文献
Ratier, Max; Pereyre, Michel; Davies, Alwyn G.; Sutcliffe, Roger
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , p. 1907 - 1916
反应条件
1: 95 percent / hydrogen / platinum oxide / diethyl ether / 760 Torr 3: 65 percent / potassium t-butoxide / dimethylsulfoxide 4: 75 percent / lithium aluminium hydride / diethyl ether / 16 h / Heating View Scheme
参考文献
Ratier, Max; Pereyre, Michel; Davies, Alwyn G.; Sutcliffe, Roger
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , p. 1907 - 1916
反应条件
sulfuric acid in nitrobenzene Pechmann reaction;
参考文献
Cisse; Kabore; Tine; Saba
Bulletin of the Chemical Society of Ethiopia, 2010 , vol. 24, # 2 p. 305 - 310
