1-(叠氮甲基)-4-甲氧基苯合成路线 （共 29 条）
反应条件
tert.-butylhydroperoxide; vanadium pentoxide in water T=100°C; 6 h;
参考文献
Tetrahedron, , vol. 67, # 44 p. 8544 - 8551
反应条件
pyridine; tert.-butylhydroperoxide; iodine in water T=20°C; 7 h; SolventReagent/catalyst;
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 14 p. 2753 - 2759
反应条件
Decaborane; palladium on activated charcoal in methanol T=20°C; 5 h; Product distribution; Further Variations:reagent amounts;
参考文献
Jung, Yeon Joo; Chang, Yu Mi; Lee, Ji Hee; Yoon, Cheol Min
Tetrahedron Letters, 2002 , vol. 43, # 48 p. 8735 - 8739
反应条件
Decaborane; palladium on activated charcoal in methanol T=20°C; 24 h; Product distribution;
参考文献
Jung, Yeon Joo; Chang, Yu Mi; Lee, Ji Hee; Yoon, Cheol Min
Tetrahedron Letters, 2002 , vol. 43, # 48 p. 8735 - 8739
反应条件
sodium azide in N,N-dimethyl-formamide
T=65°C; 4 h;
参考文献
ARYX THERAPEUTICS, INC.; LUEHR, Gary, W.; SUNDARAM, Arathi; JAISHANKAR, Priya; BHAKTA, Chhaya; DRUZGALA, Pascal
Patent: WO2010/71813 A1, 2010 ;
Location in patent: Page/Page column 111 ;
WO 2010/071813 A1
反应条件
thionyl chloride; sodium azide in N,N-dimethyl-formamide
参考文献
Wainwright, Philip; Maddaford, Adrian; Simms, Michael; Forrest, Neil; Glen, Rebecca; Hart, James; Zhang, Xiurong; Pryde, David C.; Stephenson, Peter T.; Middleton, Donald S.; Guyot, Thierry; Sutton, Scott C.
Synlett, 2011 , # 13 p. 1900 - 1904
反应条件
sodium azide; [bis(acetoxy)iodo]benzene; oxygen in acetonitrile
T=-40 - 25°C; P=760.051 Torr;
参考文献
Zhou, Wang; Zhang, Liangren; Jiao, Ning
Angewandte Chemie, International Edition, 2009 , vol. 48, # 38 p. 7094 - 7097
Angewandte Chemie, 2009 , vol. 121, # 38 p. 7228 - 7231
反应条件
trifluoromethanesulfonyl azide; sodium hydrogencarbonate; copper(II) sulfate in methanol; dichloromethane; water
T=20°C; 0.5 h;
参考文献
Beckmann, Henning S. G.; Wittmann, Valentin
Organic Letters, 2007 , vol. 9, # 1 p. 1 - 4
反应条件
sodium azide in dimethyl sulfoxide
T=20°C; 15 h; Inert atmosphere;
参考文献
Pietruszka, Joerg; Solduga, Gemma
European Journal of Organic Chemistry, 2009 , # 34 p. 5998 - 6008
反应条件
iron(III) trifluoromethanesulfonate in 1,2-dichloro-ethane
T=20°C; 2 h;
参考文献
Chan, Li Yan; Kim, Sundae; Chung, Wan Ting; Long, Chong; Kim, Sunggak
Synlett, 2011 , # 3 art. no. U09610ST, p. 415 - 419
