反应条件
in neat (no solvent) educts mixed at in vac., stirred at -30°C for 2 h; evapd. in vac., solid washed with Et2O and hexane, dissolved in toluene, filtered, concd. in vac., ppt. filtered, washed with hexane, dried in vac.;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 55, # 2 p. 504 - 512
