lithium chloride or (C2H5)3CH2C6H5NCl or n-C4H9NBr in butan-1-ol Electrolysis; (N2 or Ar); using of Sn as anode and stainless steel plate as cathode; electrolysis for 1-1.5 h with soln. of electrolyte LiCl, Bu4NBr or Et3BzNC in n-butanol; sepn. from electrolyte, washing with absolute alcohol; drying in vac.; elem. anal.;
参考文献
Russian Journal of Inorganic Chemistry, , vol. 52, # 11 p. 1682 - 1686
