in pyridine refluxing of a soln. of tetrazaporphin and Co-acetate in pyridine for 2h;;
参考文献
Berezin, B. D.; Khelevina, O. G.; Stuzhin, P. A.; Glazunov, A. V.
Russian Journal of Physical Chemistry, 1986 , vol. 60, # 9 p. 1311 - 1314
Zhurnal Fizicheskoi Khimii, 1986 , vol. 60, p. 2189 - 2193
carboxylated nitrocellulose in neat (no solvent) drop of carboxylated nitrocellulose in amyl acetate-EtOH applied to surface of aq. Co salt at 0°C for 2 h; film exposed to water vapor (35-50°C, 15 s); solidified; mounted onto Al2O3 substrate; heated at 950°C (1.33E-3 Pa); mesoscopic Co grids obtained; detd. by X-ray microanalysis;
