N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide in acetonitrile-D3
T=110°C; 0.1 h; Inert atmosphereSealed tube;
参考文献
Rueda-Becerril, Montserrat; Chatalova Sazepin, Claire; Leung, Joe C. T.; Okbinoglu, Tulin; Kennepohl, Pierre; Paquin, Jean-Francois; Sammis, Glenn M.
Journal of the American Chemical Society, 2012 , vol. 134, # 9 p. 4026 - 4029
1.1: 4-(N,N-dimethlyamino)pyridine / dichloromethane / 0.08 h / 0 °C / Inert atmosphere
1.2: 18.5 h / 0 - 20 °C / Inert atmosphere
2.1: N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide / acetonitrile-D3 / 0.1 h / 110 °C / Inert atmosphere; Sealed tube
View Scheme
参考文献
Rueda-Becerril, Montserrat; Chatalova Sazepin, Claire; Leung, Joe C. T.; Okbinoglu, Tulin; Kennepohl, Pierre; Paquin, Jean-Francois; Sammis, Glenn M.
Journal of the American Chemical Society, 2012 , vol. 134, # 9 p. 4026 - 4029
