反应条件
1: 1.) NaH / 1.) DMF, 0 deg C, 2 h, 2.) DMF, RT, 2 d
2: 89 percent / molecular sieves 4A, trimethylamine-borane, AlCl3 / tetrahydrofuran / 5 h / Ambient temperature
3: pyridine / CH2Cl2
4: LiN3 / dimethylformamide / Ambient temperature
View Scheme
参考文献
Sakairi, Nobuo; Takahashi, Shunya; Wang, Feng; Ueno, Yoshihito; Kuzuhara, Hiroyoshi
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 6 p. 1756 - 1758
