4-(2,6-二甲基苯基)-3-氨基硫脲合成路线 (共 5 条)
反应条件
1: With sodium hydroxide in N,N-dimethyl-formamide T=20°C; 1 h; 2: With hydrazine hydrate in N,N-dimethyl-formamide T=60°C; 1 h;
参考文献
Jung, Michael E.; Chamberlain, Brian T.; Ho, Chi-Lee C.; Gillespie, Eugene J.; Bradley, Kenneth A.
ACS Medicinal Chemistry Letters, 2014 , vol. 5, # 4 p. 363 - 367
反应条件
hydrazine hydrate in ethanol T=80°C; 1 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 19, # 4 p. 1152 - 1154
反应条件
1: NH4OH / aq. ethanol / 1 h / 30 °C 3: 50percent hydrazine hydrate View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 61, # 2 p. 168 - 169
反应条件
2: 50percent hydrazine hydrate View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 61, # 2 p. 168 - 169
反应条件
hydrogenchloride; sodium nitrate in water
T=10 - 15°C; 0.666667 h;
参考文献
Cowper; Astik; Thaker
Journal of the Indian Chemical Society, 1981 , vol. 58, # 11 p. 1087 - 1088