2,2'-联吡啶-4,4'-二甲酸甲酯合成路线 （共 11 条）
反应条件
sulfuric acid 60 h; Heating;
参考文献
Miyoshi, Daisuke; Karimata, Hisae; Wang, Zhong-Ming; Koumoto, Kazuya; Sugimoto, Naoki
Journal of the American Chemical Society, 2007 , vol. 129, # 18 p. 5919 - 5925
反应条件
1: 50 percent / aq. H2SO4; KMnO4 / 12 h / Heating 2: 99 percent / conc. H2SO4 / 60 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 129, # 18 p. 5919 - 5925
反应条件
1: FeCl3 2: KMnO4; H2O 3: H2SO4 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 68, p. 2574,2576
反应条件
1: bromine; aqueous sodium nitrite solution; aqueous hydrobromic acid 2: copper / 240 °C 3: KMnO4; H2O 4: H2SO4 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 68, p. 2574,2576
反应条件
1: copper / 240 °C 2: KMnO4; H2O 3: H2SO4 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 68, p. 2574,2576
反应条件
1: 4,4'-dimethyl-2,2'-bipyridine With chromium(VI) oxide; sulfuric acid T=0 - 80°C; 2: methanol With sulfuric acid Reflux;
参考文献
Ohkanda, Junko; Satoh, Ritsuko; Kato, Nobuo
Chemical Communications, 2009 , # 45 p. 6949 - 6951
反应条件
1: nitric acid / 2 h / |Reflux 2: thionyl chloride / 20 h / |Reflux View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 38 p. 9956 - 9960
Angew. Chem.,
反应条件
1: 72 percent / sodium borohydride / ethanol 2: 60 percent / MnO2 (activated) / dioxane View Scheme
参考文献
Ciana, Leopoldo Della; Dressick, Walter J.; Zelewsky, A. von
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 2 p. 163 - 165
反应条件
sodium hydroxide in methanol Reflux;
参考文献
Ohkanda, Junko; Satoh, Ritsuko; Kato, Nobuo
Chemical Communications, 2009 , # 45 p. 6949 - 6951
反应条件
sodium tetrahydroborate in ethanol Reflux;
参考文献
Tetrahedron Asymmetry, , vol. 24, # 8 p. 515 - 525
