2,2,2-三氯月桂酸乙酯合成路线 (共 3 条)
反应条件
sodium tetrahydroborate; selenium in N,N-dimethyl-formamide T=40 - 50°C; 1 h;
参考文献
Huang, Zhi-Zhen; Zhou, Xun-Jun
Synthesis, 1989 , # 9 p. 693 - 694
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 2.5 h; Heating;
参考文献
Ram, Ram N.; Meher, Nabin Kumar
Organic Letters, 2003 , vol. 5, # 2 p. 145 - 147
反应条件
1: (1'-14C)-dodecanoic acid With thionyl chloride
3 h;
2: 2,2,2-trichloroethyl alcohol With triethylamine in dichloromethane
T=20°C; 8 h; Further stages.;
参考文献
Ram, Ram N.; Meher, Nabin Kumar
Organic Letters, 2003 , vol. 5, # 2 p. 145 - 147