2,2,2-三氟-4-甲氧基乙酰苯合成路线 （共 42 条）
反应条件
1: (trifluoromethyl)-trimethylsilane With silver monofluoride in various solvent(s) T=20°C; 2 h; 2: 4-methoxy-benzoyl chloride in various solvent(s) T=20°C; 12 h; Further stages.;
参考文献
Kremlev, Mikhail M.; Mushta, Aleksej I.; Tyrra, Wieland; Naumann, Dieter; Fischer, Hendrik T.M.; Yagupolskii, Yurii L.
Journal of Fluorine Chemistry, 2007 , vol. 128, # 11 p. 1385 - 1389
反应条件
Co(III) ortho-phenylene-bis(N'-methyloxamidate); oxygen; pivalaldehyde in dichloromethane
参考文献
Blay, Gonzalo; Fernandez, Isabel; Marco-Aleixandre, Alicia; Monje, Belen; Pedro, Jose R; Ruiz, Rafael
Tetrahedron, 2002 , vol. 58, # 42 p. 8565 - 8571
反应条件
aluminium trichloride in dichloromethane T=0°C; 4 h;
参考文献
Keumi, Takashi; Shimada, Masakazu; Takahashi, Masahiro; Kitajima, Hidehiko
Chemistry Letters, 1990 , # 5 p. 783 - 786
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane 48 h; Ambient temperature;
参考文献
Journal of Fluorine Chemistry, , vol. 56, # 2 p. 215 - 237
反应条件
4-(N,N-dimethlyamino)pyridine; bis(trifluoromethyl)cadmium*glyme in dichloromethane 48 h; Ambient temperature;
参考文献
Journal of Fluorine Chemistry, , vol. 56, # 2 p. 215 - 237
反应条件
aluminium trichloride in dichloromethane 15 h; Ambient temperature;
参考文献
Simchen, Gerhard; Schmidt, Andreas
Synthesis, 1996 , # 9 p. 1093 - 1094
反应条件
tetrasulphur tetranitride in toluene 23 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 33, # 2 p. 295 - 302
反应条件
1: With tetra-n-butylammonium acetate in toluene T=0 - 20°C; 1 h; 2: With hydrogenchloride in tetrahydrofuran; toluene
参考文献
Kawano, Yoshikazu; Kaneko, Nobuya; Mukaiyama, Teruaki
Bulletin of the Chemical Society of Japan, 2006 , vol. 79, # 7 p. 1133 - 1145
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-78°C; 2.5 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 135, # 14 p. 5364 - 5367
反应条件
(i) Mg, Et2O, (ii) /BRN= 746197/; Multistep reaction;
参考文献
Journal of medicinal chemistry, , vol. 9, # 2 p. 176 - 178
