2,3-二甲基-1(2H)-异喹啉酮合成路线 (共 9 条)
参考文献
Chemische Berichte, , vol. 25, p. 3565
反应条件
potassium hydroxide in water
10 h; Heating;
参考文献
Kost, A. N.; Terenin, V. I.; Yudin, L. G.; Sagitullin, R. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , p. 965 - 969
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , vol. 16, # 9 p. 1272 - 1277
反应条件
T=100°C; Behandeln einer wss. Loesung des Reaktionsprodukts mit Kalium-hexacyanoferrat(III) und wss. Kalilauge.;
参考文献
Brooker; White
Journal of the American Chemical Society, 1951 , vol. 73, p. 1094,1096
反应条件
n-butyllithium
1.) THF, ether, reflux, 45 min; 2.) room temp., 1 h; Yield given. Multistep reaction;
参考文献
Mali, R. S.; Kulkarni, B. K.; Shankaran, K.
Synthesis, 1982 , # 4 p. 329 - 330
反应条件
potassium tert-butylate
liquid NH3, 2.) 3 h, irradiation; Yield given. Multistep reaction;
参考文献
Beugelmans; Bois-Choussy
Synthesis, 1981 , vol. No.9, p. 729 - 731
反应条件
potassium tert-butylate
liquid NH3, 2.) 5 h, irradiation; Yield given. Multistep reaction;
参考文献
Beugelmans; Bois-Choussy
Synthesis, 1981 , vol. No.9, p. 729 - 731
反应条件
dilithium tetrachloropalladate
1.) CH3CN, 25 deg C, 16 h; 2.) 80 deg C, 5 h; Yield given. Multistep reaction;
参考文献
Larock, R.C.; Liu, C.-L.; Lau, H. H.; Varaprath, S.
Tetrahedron Letters, 1984 , vol. 25, # 40 p. 4459 - 4462
反应条件
in ethanol
T=150°C; 30 h; other solvents; other temperatures; other time. Other nucleophiles (OH(1-)); Product distributionMechanism;
参考文献
Kost, A. N.; Terenin, V. I.; Yudin, L. G.; Sagitullin, R. S.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , p. 965 - 969
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , vol. 16, # 9 p. 1272 - 1277
参考文献
Gabriel; Neumann
Chemische Berichte, 1892 , vol. 25, p. 3565