1: SOCl2 View Scheme

暂无反应条件数据

durch Ueberfuehrung in das Chlorid und Behandeln mit Methanol;

1: sodium hydride / tetrahydrofuran / 6 h / -30 °C 2: thionyl chloride / dichloromethane / 4 h / 0 °C / |Inert atmosphere; |Reflux 3: triethylamine / 3 h / 0 - 20 °C 4: dihydrogen peroxide; Na2WO4·2H2O / methanol; water / 12 h / 20 °C 5: sodium hydride / N,N-dimethyl-formamide / 1.5 h / 0 - 20 °C 6: tetrahydrofuran / 3 h / 0 - 20 °C / |Inert atmosphere 7: N-iodo-succinimide / water; 1,4-dioxane / 36 h / 30 °C View Scheme

thionyl chloride 3 h; Heating / reflux;

borane in tetrahydrofuran; water

Davy reagent

T=76°C; Kinetics;