3-甲基-3-乙烯基-1-环丙烯合成路线 （共 3 条）
反应条件
potassium tert-butylate in dimethyl sulfoxide
T=40°C; 2 h;
参考文献
Bolesov, I. G.; Ignatchenko, A. V.; Bovin, N. V.; Prudchenko, I. A.; Surmina, L. S.; et al.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 1.2 p. 87 - 100
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 1 p. 102 - 119
反应条件
1: 68 percent / 50percent NaOH / triethylbenzylammonium chloride / ethanol / 16 h / 25 °C
2: 18 percent / Zn, conc. HCl / ethanol / 10 - 15 °C
3: 50 percent / potassium tert-butoxide / dimethylsulfoxide / 2 h / 40 °C
View Scheme
参考文献
Bolesov, I. G.; Ignatchenko, A. V.; Bovin, N. V.; Prudchenko, I. A.; Surmina, L. S.; et al.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 1.2 p. 87 - 100
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 1 p. 102 - 119
反应条件
1: 18 percent / Zn, conc. HCl / ethanol / 10 - 15 °C
2: 50 percent / potassium tert-butoxide / dimethylsulfoxide / 2 h / 40 °C
View Scheme
参考文献
Bolesov, I. G.; Ignatchenko, A. V.; Bovin, N. V.; Prudchenko, I. A.; Surmina, L. S.; et al.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 1.2 p. 87 - 100
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 1 p. 102 - 119
