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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-异丙基联苯
合成路线
（共 38 条）
1190929-69-1
→
反应条件
7116-95-2
4-异丙基联苯
反应条件
methanol; palladium 10 on activated carbon; hydrogen T=20°C; P=760.051 Torr; 24 h; Inert atmosphere;
参考文献
Wilsily, Ashraf; Nguyen, Yen; Fillion, Eric
Journal of the American Chemical Society, 2009 , vol. 131, # 43 p. 15606 - 15607
2621-46-7
1-氯-4-丙-2-基苯
+
98-80-6
苯硼酸
→
反应条件
7116-95-2
4-异丙基联苯
反应条件
3,3'-(3,4-bis(dichloromethylene)cyclobut-1-ene-1,2-diyl)bis(1-methyl-1H-imidazolium) bis(tetrafluoroborate); palladium diacetate; sodium t-butanolate in toluene T=20°C; Suzuki-Miyaura coupling; 1 h; Inert atmosphere;
参考文献
Rahimi, Alireza; Papai, Imre; Madarasz, Udam; Gjikaj, Mimoza; Namyslo, Jan C.; Schmidt, Andreas
European Journal of Organic Chemistry, 2012 , # 4 p. 754 - 763
34352-74-4
2-(4-联苯基)-2-丙醇
→
反应条件
7116-95-2
4-异丙基联苯
反应条件
ethanol; copper oxide-chromium oxide T=225°C; P=62518.2 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 77, p. 1769,1773
92-52-4
联苯
+
187737-37-7
→
反应条件
7116-95-2
4-异丙基联苯
+
18970-30-4
4,4'-二异丙基联苯
+
61434-46-6
+
20282-30-8
3-异丙基联苯
+
69375-12-8
反应条件
MOR(97) in decalin T=220°C; P=7600.51 Torr; Product distribution / selectivity;
参考文献
GENERAL ELECTRIC COMPANY
Patent: EP1533288 A2, 2005 ;
Location in patent: Page/Page column 9-10 ;
92-66-0
4-溴代联苯
+
77047-87-1
2-丙基溴化锌
→
反应条件
7116-95-2
4-异丙基联苯
反应条件
CPhos; palladium diacetate in tetrahydrofuran T=0 - 20°C; Negishi coupling reaction; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 131, p. 7532 - 7533
108-86-1
溴代苯
+
17356-09-1
1-碘-4-异丙苯
→
反应条件
7116-95-2
4-异丙基联苯
反应条件
1: bromobenzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; Negishi coupling reaction; 0.166667 h; Inert atmosphere; 2: With zinc(II) chloride in tetrahydrofuran; hexane T=-78 - 20°C; Negishi coupling reaction; Inert atmosphere; 3: 4-isopropyl-iodobenzene With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran; hexane T=60°C; Negishi coupling reaction; 2 h; Inert atmosphere;
参考文献
Liu, Qiang; Lan, Yu; Liu, Jing; Li, Gang; Wu, Yun-Dong; Lei, Aiwen
Journal of the American Chemical Society, 2009 , vol. 131, # 29 p. 10201 - 10210
92-52-4
联苯
+
187737-37-7
→
反应条件
反应条件
silica-alumina T=300°C; P=7500.75 Torr; Autoclave; Reagent/catalystTime;
参考文献
Applied Catalysis A: General, , vol. 453, p. 195 - 203
17356-09-1
1-碘-4-异丙苯
+
71-43-2
苯
→
反应条件
7116-95-2
4-异丙基联苯
反应条件
potassium tert-butylate; N-methyl-2-(methylamino)ethylamine T=80°C; sealed tubeInert atmosphere;
参考文献
Liu, Wei; Cao, Hao; Zhang, Hua; Zhang, Heng; Chung, Kin Ho; He, Chuan; Wang, Haibo; Kwong, Fuk Yee; Lei, Aiwen
Journal of the American Chemical Society, 2010 , vol. 132, # 47 p. 16737 - 16740
92-66-0
4-溴代联苯
+
1068-55-9
异丙基氯化镁
→
反应条件
7116-95-2
4-异丙基联苯
反应条件
1: isopropylmagnesium chloride With bis(acetylacetonate)nickel(II); 1-(2-carboxyethyl)-3-mesityl-1H-imidazol-3-ium chloride; lithium tert-butylate in tetrahydrofuran T=0°C; 0.166667 h; Inert atmosphere; 2: 4-bromo-1,1'-biphenyl in tetrahydrofuran T=0 - 20°C; Kumada-Corriu-Tamao type reaction; Inert atmosphere;
参考文献
Lohre, Claudia; Droege, Thomas; Wang, Congyang; Glorius, Frank
Chemistry - A European Journal, 2011 , vol. 17, # 22 p. 6052 - 6055
92-91-1
联苯单乙酮
→
反应条件
7116-95-2
4-异丙基联苯
反应条件
1: diethyl ether / 72 h / Ambient temperature 2: AlCl3 / cyclohexene / 72 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 17 p. 4656 - 4661
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