反应条件
1: 1.) sodium azide, trifluoroacetic acid, 2. ) LAH / 1.) CHCl3, room temperature, 4 h, 2.) ether, reflux, 3 h 2: 86 percent / K2CO3 / dimethylformamide / 48 h / 60 °C View Scheme
参考文献
Costa, Brian R. de; George, Clifford; Burke, Terrence R.; Rafferty, Michael F.; Contreras, Patricia C.; et al.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 8 p. 1571 - 1575
