1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
T=0°C; 3 h; Title compound not separated from byproducts.;
参考文献
Pierik, Antonio J.; Ciceri, Daniele; Broeker, Gerd; Edwards, Christopher H.; McFarlane, William; Winter, Joachim; Buckel, Wolfgang; Golding, Bernard T.
Journal of the American Chemical Society, 2002 , vol. 124, # 47 p. 14039 - 14048
1: 77 percent / NBS; KO-tBu / 2-methyl-propan-2-ol / 40 h / 35 °C
2: DBU / tetrahydrofuran / 3 h / 0 °C
View Scheme
参考文献
Pierik, Antonio J.; Ciceri, Daniele; Broeker, Gerd; Edwards, Christopher H.; McFarlane, William; Winter, Joachim; Buckel, Wolfgang; Golding, Bernard T.
Journal of the American Chemical Society, 2002 , vol. 124, # 47 p. 14039 - 14048
1: 88 percent / EtONa / ethanol / 3 h / Heating
2: 77 percent / NBS; KO-tBu / 2-methyl-propan-2-ol / 40 h / 35 °C
3: DBU / tetrahydrofuran / 3 h / 0 °C
View Scheme
参考文献
Pierik, Antonio J.; Ciceri, Daniele; Broeker, Gerd; Edwards, Christopher H.; McFarlane, William; Winter, Joachim; Buckel, Wolfgang; Golding, Bernard T.
Journal of the American Chemical Society, 2002 , vol. 124, # 47 p. 14039 - 14048
1: 88 percent / EtONa / ethanol / 3 h / Heating
2: 77 percent / NBS; KO-tBu / 2-methyl-propan-2-ol / 40 h / 35 °C
3: DBU / tetrahydrofuran / 3 h / 0 °C
View Scheme
参考文献
Pierik, Antonio J.; Ciceri, Daniele; Broeker, Gerd; Edwards, Christopher H.; McFarlane, William; Winter, Joachim; Buckel, Wolfgang; Golding, Bernard T.
Journal of the American Chemical Society, 2002 , vol. 124, # 47 p. 14039 - 14048
