2-氨基-4-羟基蝶啶-6-甲醛合成路线 （共 22 条）
反应条件
formic acid T=20°C; 0.5 h;
参考文献
Freisleben, Achim; Schieberle, Peter; Rychlik, Michael
Journal of Agricultural and Food Chemistry, 2002 , vol. 50, # 17 p. 4760 - 4768
反应条件
hydrogenchloride in 1,4-dioxane 0.5 h; Heating;
参考文献
Taylor, Edward C.; Ray, Partha S.
Synthetic Communications, 1987 , vol. 17, # 16 p. 1865 - 1868
反应条件
oxygen in water T=20°C; pH=7; 0.25 h; Irradiation;
参考文献
Organic and Biomolecular Chemistry, , vol. 8, # 4 p. 800 - 810
反应条件
hydrogen bromide T=100°C; 2 h;
参考文献
Journal of Medicinal Chemistry, , vol. 44, # 9 p. 1364 - 1371
反应条件
potassium meta-periodate
参考文献
Journal of the Chemical Society, , p. 79,83
US2541717 , ;
DE839498 , ;
DRP/DRBP Org.Chem.
Chemische Berichte, , vol. 82, p. 25,30
US2603643 , ;
反应条件
1: 86.5 percent / MeONa / methanol / 18 h / 70 °C 2: 92.1 percent / 5 percent aq. NaOH / 0.17 h / Heating 3: 100 percent / aq. formic acid / 0.5 h / 20 °C View Scheme
参考文献
Journal of Agricultural and Food Chemistry, , vol. 50, # 17 p. 4760 - 4768
参考文献
Photochemistry and Photobiology, , vol. 85, # 1 p. 365 - 373
反应条件
1: 76 percent / palladium acetate, tri-o-tolylphosphine, copper(I) iodide, triethylamine / acetonitrile / 18 h / Heating 2: 92 percent / 1.) ozone, 2.) methyl sulfide / CH2Cl2 / 1.) -78 deg C, 10 min, 2.) RT, 0.5 h 3: 88 percent / aq. hydrochloric acid / dioxane / 0.5 h / Heating View Scheme
参考文献
Synthetic Communications, , vol. 17, # 16 p. 1865 - 1868
反应条件
1: 92 percent / 1.) ozone, 2.) methyl sulfide / CH2Cl2 / 1.) -78 deg C, 10 min, 2.) RT, 0.5 h 2: 88 percent / aq. hydrochloric acid / dioxane / 0.5 h / Heating View Scheme
参考文献
Synthetic Communications, , vol. 17, # 16 p. 1865 - 1868
反应条件
oxygen T=20°C; PhotolysisDarkness;
参考文献
Photochemistry and Photobiology, , vol. 85, # 1 p. 365 - 373
