2-氨基-4-羟基蝶啶-6-甲醛合成路线 （共 22 条）
反应条件
1: 92.1 percent / 5 percent aq. NaOH / 0.17 h / Heating 2: 100 percent / aq. formic acid / 0.5 h / 20 °C View Scheme
参考文献
Journal of Agricultural and Food Chemistry, , vol. 50, # 17 p. 4760 - 4768
反应条件
air in water T=20°C; pH=7; Irradiation; Quantum yield; pH-valueReagent/catalyst;
参考文献
Journal of Photochemistry and Photobiology A: Chemistry, , vol. 209, # 2-3 p. 104 - 110
反应条件
oxygen in water T=20°C; pH=7; Irradiation; Quantum yieldKineticsMechanism; Reagent/catalystWavelengthTimeConcentration;
参考文献
Organic and Biomolecular Chemistry, , vol. 8, # 4 p. 800 - 810
反应条件
bromine; sodium acetate; acetic acid; nickel dichloride 1.) 95-100 deg C, 10 h, 2.) reflux, 1 h; Yield given. Multistep reaction;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 30, # 7 p. 1358 - 1359
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 7 p. 1669 - 1670
反应条件
oxygen; rose bengal in water-d2 pH=10.5; Irradiation; Kinetics;
参考文献
Photochemistry and Photobiology, , vol. 83, # 3 p. 526 - 534
反应条件
in water T=20°C; pH=5.5; UV-irradiation; Quantum yield;
参考文献
Helvetica Chimica Acta, , vol. 89, # 6 p. 1090 - 1104
反应条件
hydrogenchloride Heating; Product distribution;
参考文献
Journal of Heterocyclic Chemistry, , vol. 21, p. 909
反应条件
potassium hydroxide; potassium permanganate
参考文献
Zav'yalov, S. I.; Zavozin, A. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 7 p. 1358 - 1359
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 7 p. 1669 - 1670
参考文献
Waller et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 4630,4632
反应条件
1: 83 percent / 4 h / 130 °C 2: 262 mg / 0.25 h / 120 - 125 °C / 0.01 Torr 3: 118 mg / sodium borohydride / ethanol / 45 °C 4: 81 mg / NaOH / 80 °C View Scheme
参考文献
Freisleben, Achim; Schieberle, Peter; Rychlik, Michael
Journal of Agricultural and Food Chemistry, 2002 , vol. 50, # 17 p. 4760 - 4768
