1,4-二甲基-2,5-二硝基苯合成路线 （共 14 条）
反应条件
1: nitric acid / 170 °C
2: hydrogen chloride
3: tin; alcohol; hydrochloric acid
View Scheme
参考文献
Haeussermann; Martz
Chemische Berichte, 1893 , vol. 26, p. 2983
Chemische Berichte, 1895 , vol. 28, p. 81
反应条件
chromium(VI) oxide; sulfuric acid
T=25°C; 1 h;
参考文献
Arya, Dev P.; Jebaratnam, David J.
Tetrahedron Letters, 1995 , vol. 36, # 25 p. 4369 - 4372
反应条件
1: 78 percent / dimethylformamide / 90 - 120 °C
2: 50 percent / H2 / 10percent Pd-C / ethyl acetate / 760 Torr / Ambient temperature
View Scheme
参考文献
Berlin, A.; Bradamante, S.; Ferraccioli, R.; Pagani, G. A.; Sannicolo, F.
Journal of the Chemical Society, Chemical Communications, 1987 , # 15 p. 1176 - 1177
反应条件
1: Br2 / Irradiation
2: (i) KOH, (ii) aq. H2O2, AcOH, (iii) (pyrolysis)
View Scheme
参考文献
Staab,H.A.; Haffner,H.
Chemische Berichte, 1977 , vol. 110, p. 3358 - 3365
