二锂4-氨基-N-[3-(乙烯基磺酰)苯基]萘酰亚胺-3,6-二磺酸合成路线 (共 7 条)
反应条件
1: fuming H2SO4 / 3 h / 90 °C 2: 1.) aq. KOH, 2.) aq. HCl / 1) pH 12.5, 50 deg C, 10 min; 2) pH 2.0, 50 deg C, 10 min; 3) pH 2, 3 d, room temperature 3: 79 percent / H2O / 48 h 4: 1.) aq. H2SO4, 2.) aq. KCl / 1) 4 deg C, 24 h; 2) 50 deg C 5: 97 percent / aq. NaOH / 0.25 h / Ambient temperature; pH 10 6: 8.95 g / Dowex 50W-X2 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 103, # 25 p. 7615 - 7620
反应条件
1: 79 percent / H2O / 48 h 2: 1.) aq. H2SO4, 2.) aq. KCl / 1) 4 deg C, 24 h; 2) 50 deg C 3: 97 percent / aq. NaOH / 0.25 h / Ambient temperature; pH 10 4: 8.95 g / Dowex 50W-X2 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 103, # 25 p. 7615 - 7620
反应条件
1: 79 percent / H2O / 48 h 2: 1.) aq. H2SO4, 2.) aq. KCl / 1) 4 deg C, 24 h; 2) 50 deg C 3: 97 percent / aq. NaOH / 0.25 h / Ambient temperature; pH 10 4: 8.95 g / Dowex 50W-X2 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 103, # 25 p. 7615 - 7620
反应条件
1: 1.) aq. KOH, 2.) aq. HCl / 1) pH 12.5, 50 deg C, 10 min; 2) pH 2.0, 50 deg C, 10 min; 3) pH 2, 3 d, room temperature 2: 79 percent / H2O / 48 h 3: 1.) aq. H2SO4, 2.) aq. KCl / 1) 4 deg C, 24 h; 2) 50 deg C 4: 97 percent / aq. NaOH / 0.25 h / Ambient temperature; pH 10 5: 8.95 g / Dowex 50W-X2 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 103, # 25 p. 7615 - 7620
参考文献
Stewart, Walter W.
Journal of the American Chemical Society, 1981 , vol. 103, # 25 p. 7615 - 7620
反应条件
1: 1.) aq. H2SO4, 2.) aq. KCl / 1) 4 deg C, 24 h; 2) 50 deg C 2: 97 percent / aq. NaOH / 0.25 h / Ambient temperature; pH 10 3: 8.95 g / Dowex 50W-X2 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 103, # 25 p. 7615 - 7620
反应条件
1: 97 percent / aq. NaOH / 0.25 h / Ambient temperature; pH 10 2: 8.95 g / Dowex 50W-X2 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 103, # 25 p. 7615 - 7620