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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
7124-49-4
合成路线
（共 15 条）
49598-85-8
小柱孢酮
→
反应条件
7124-49-4
反应条件
sodium hydroxide T=45°C;
参考文献
Ichinose; Ebizuka; Sankawa
Chemical and Pharmaceutical Bulletin, 2001 , vol. 49, # 2 p. 192 - 196
2150-44-9
3,5-二羟基苯甲酸甲酯
→
反应条件
7124-49-4
反应条件
1.1: 96 percent / K2CO3 / acetone / 12 h / Heating 2.1: 97 percent / LiAlH4 3.1: 84 percent / Et3N / CH2Cl2 / 0.33 h / 4 °C 4.1: 69 percent / benzyltriethylammonium chloride / H2O; CHCl3 / 2 h / Heating 5.1: 92 percent / aq. Ba(OH)2 / dioxane / 15 h / 115 °C 6.1: 99 percent / AcOH; 60 percent aq. HClO4 / 0.08 h / 35 °C 7.1: 97 percent / H2 / 5 percent Pd/C / ethanol 8.1: MeONa / methanol / 0.33 h / 60 °C 8.2: 20 percent / NaBH4 / methanol / 4 h / 60 °C 9.1: 76 percent / 1N NaOH / 3 h / 45 °C View Scheme
参考文献
Ichinose; Ebizuka; Sankawa
Chemical and Pharmaceutical Bulletin, 2001 , vol. 49, # 2 p. 192 - 196
58605-10-0
3,5-二苄氧基苯甲酸甲酯
→
反应条件
7124-49-4
反应条件
1.1: 97 percent / LiAlH4 2.1: 84 percent / Et3N / CH2Cl2 / 0.33 h / 4 °C 3.1: 69 percent / benzyltriethylammonium chloride / H2O; CHCl3 / 2 h / Heating 4.1: 92 percent / aq. Ba(OH)2 / dioxane / 15 h / 115 °C 5.1: 99 percent / AcOH; 60 percent aq. HClO4 / 0.08 h / 35 °C 6.1: 97 percent / H2 / 5 percent Pd/C / ethanol 7.1: MeONa / methanol / 0.33 h / 60 °C 7.2: 20 percent / NaBH4 / methanol / 4 h / 60 °C 8.1: 76 percent / 1N NaOH / 3 h / 45 °C View Scheme
参考文献
Ichinose; Ebizuka; Sankawa
Chemical and Pharmaceutical Bulletin, 2001 , vol. 49, # 2 p. 192 - 196
24131-31-5
3,5-二苄氧基苯甲醇
→
反应条件
7124-49-4
反应条件
1.1: 84 percent / Et3N / CH2Cl2 / 0.33 h / 4 °C 2.1: 69 percent / benzyltriethylammonium chloride / H2O; CHCl3 / 2 h / Heating 3.1: 92 percent / aq. Ba(OH)2 / dioxane / 15 h / 115 °C 4.1: 99 percent / AcOH; 60 percent aq. HClO4 / 0.08 h / 35 °C 5.1: 97 percent / H2 / 5 percent Pd/C / ethanol 6.1: MeONa / methanol / 0.33 h / 60 °C 6.2: 20 percent / NaBH4 / methanol / 4 h / 60 °C 7.1: 76 percent / 1N NaOH / 3 h / 45 °C View Scheme
参考文献
Ichinose; Ebizuka; Sankawa
Chemical and Pharmaceutical Bulletin, 2001 , vol. 49, # 2 p. 192 - 196
2732-96-9
3,5-二苄氧基苯甲酸甲酯
→
反应条件
7124-49-4
反应条件
1.1: 99 percent / AcOH; 60 percent aq. HClO4 / 0.08 h / 35 °C 2.1: 97 percent / H2 / 5 percent Pd/C / ethanol 3.1: MeONa / methanol / 0.33 h / 60 °C 3.2: 20 percent / NaBH4 / methanol / 4 h / 60 °C 4.1: 76 percent / 1N NaOH / 3 h / 45 °C View Scheme
参考文献
Ichinose; Ebizuka; Sankawa
Chemical and Pharmaceutical Bulletin, 2001 , vol. 49, # 2 p. 192 - 196
58604-84-5
→
反应条件
7124-49-4
反应条件
1.1: 92 percent / aq. Ba(OH)2 / dioxane / 15 h / 115 °C 2.1: 99 percent / AcOH; 60 percent aq. HClO4 / 0.08 h / 35 °C 3.1: 97 percent / H2 / 5 percent Pd/C / ethanol 4.1: MeONa / methanol / 0.33 h / 60 °C 4.2: 20 percent / NaBH4 / methanol / 4 h / 60 °C 5.1: 76 percent / 1N NaOH / 3 h / 45 °C View Scheme
参考文献
Ichinose; Ebizuka; Sankawa
Chemical and Pharmaceutical Bulletin, 2001 , vol. 49, # 2 p. 192 - 196
79762-35-9
→
反应条件
7124-49-4
反应条件
1.1: 99 percent / AcOH; 60 percent aq. HClO4 / 0.08 h / 35 °C 2.1: 97 percent / H2 / 5 percent Pd/C / ethanol 3.1: MeONa / methanol / 0.33 h / 60 °C 3.2: 20 percent / NaBH4 / methanol / 4 h / 60 °C 4.1: 76 percent / 1N NaOH / 3 h / 45 °C View Scheme
参考文献
Ichinose; Ebizuka; Sankawa
Chemical and Pharmaceutical Bulletin, 2001 , vol. 49, # 2 p. 192 - 196
65857-78-5
→
反应条件
7124-49-4
反应条件
1.1: 97 percent / H2 / 5 percent Pd/C / ethanol 2.1: MeONa / methanol / 0.33 h / 60 °C 2.2: 20 percent / NaBH4 / methanol / 4 h / 60 °C 3.1: 76 percent / 1N NaOH / 3 h / 45 °C View Scheme
参考文献
Ichinose; Ebizuka; Sankawa
Chemical and Pharmaceutical Bulletin, 2001 , vol. 49, # 2 p. 192 - 196
80457-61-0
→
反应条件
7124-49-4
反应条件
1.1: 69 percent / benzyltriethylammonium chloride / H2O; CHCl3 / 2 h / Heating 2.1: 92 percent / aq. Ba(OH)2 / dioxane / 15 h / 115 °C 3.1: 99 percent / AcOH; 60 percent aq. HClO4 / 0.08 h / 35 °C 4.1: 97 percent / H2 / 5 percent Pd/C / ethanol 5.1: MeONa / methanol / 0.33 h / 60 °C 5.2: 20 percent / NaBH4 / methanol / 4 h / 60 °C 6.1: 76 percent / 1N NaOH / 3 h / 45 °C View Scheme
参考文献
Ichinose; Ebizuka; Sankawa
Chemical and Pharmaceutical Bulletin, 2001 , vol. 49, # 2 p. 192 - 196
18512-30-6
萘-1,3,6,8-四酚
→
反应条件
7124-49-4
反应条件
1.1: MeONa / methanol / 0.33 h / 60 °C 1.2: 25 percent / NaBH4 / methanol / 4 h / 60 °C 2.1: 76 percent / 1N NaOH / 3 h / 45 °C View Scheme
参考文献
Ichinose; Ebizuka; Sankawa
Chemical and Pharmaceutical Bulletin, 2001 , vol. 49, # 2 p. 192 - 196
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