4,5-二氢-2-苯基恶唑合成路线 (共 96 条)
反应条件
1: benzamide With sodium hydroxide in dimethyl sulfoxide T=20°C; 0.5 h; 2: (2-bromoethyl)(diphenyl)sulfonium trifluoromethanesulfonate With potassium iodide in dimethyl sulfoxide T=20°C; 2 h;
参考文献
Yamanaka, Hiroyuki; Yamane, Yoshinobu; Mukaiyama, Teruaki
Heterocycles, 2004 , vol. 63, # 12 p. 2813 - 2826
反应条件
1,2,2-trichloro-1,1,2-trichloro-ethane; 2-mercaptoethanamine hydrochloride; triethylamine; benzoic acid in dichloromethane T=22°C;
参考文献
Tetrahedron, , vol. 49, # 41 p. 9353 - 9372
反应条件
[bis(acetoxy)iodo]benzene in acetonitrile T=20°C; 3 h;
参考文献
Synlett, , # 12 p. 1921 - 1924
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 16.0833 h; Inert atmosphere;
参考文献
Petersson, Maria J.; Jenkins, Ian D.; Loughlin, Wendy A.
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 4 p. 739 - 746
反应条件
in acetonitrile RT, 2 h, then reflux, 6 h;
参考文献
Singh, Harjit; Sarin, Rakesh
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 81 - 82
反应条件
2: 50 percent / P2O5 / benzene / Heating View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 23, # 9 p. 857 - 859
反应条件
1: 160 - 200 °C 2: P2O5 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 57, p. 1079
参考文献
Chemische Berichte, , vol. 23, p. 2502
反应条件
tetra-n-butylammonium perchlorate in tetrahydrofuran electrochemical reduction;
参考文献
Bulletin de la Societe Chimique de France, , # 44 p. 537 - 543
反应条件
aluminum oxide 0.0833333 h; Irradiation;
参考文献
Oussaid; Berlan; Soufiaoui; Garrigues
Synthetic Communications, 1995 , vol. 25, # 5 p. 659 - 665