(2E)-3-(3,4,5-三甲氧基苯基)丙烯醛合成路线 (共 2 条)
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=20°C; 6 h; 2: in tetrahydrofuran; water T=10 - 15°C; pH=5; Acidic aqueous solution;
参考文献
Spangler, Brenda D.; Spangler, Charles W.; Tarter, E. Scott
Patent: US2009/43109 A1, 2009 ;
Location in patent: Page/Page column sheet 4; 11 ;
反应条件
amberlyst-15; 2,3-dicyano-5,6-dichloro-p-benzoquinone in toluene T=110°C; 0.583333 h; microwave irradiation;
参考文献
Sinha, Arun K.; Sharma, Anuj; Swaroop, Anand; Kumar, Vinod
Tetrahedron, 2007 , vol. 63, # 4 p. 1000 - 1007