water; oxygen; copper(l) iodide; palladium dichloride in N,N-dimethyl-formamide
T=50°C; Wacker oxidation; 24 h; Title compound not separated from byproducts.;
参考文献
Gaunt; Yu; Spencer
Chemical Communications, 2001 , # 18 p. 1844 - 1845
1: With PyBH2I in dichloromethane
T=20°C;
2: With sodium hydroxide; dihydrogen peroxide in methanol; dichloromethane
T=0 - 20°C; Title compound not separated from byproducts;
参考文献
Clay, Julia M.; Vedejs, Edwin
Journal of the American Chemical Society, 2005 , vol. 127, # 16 p. 5766 - 5767