1-硝基-4-(三氟甲氧基)苯合成路线 (共 5 条)
反应条件
Bi(NO3)3·5H2O in toluene T=120°C; 0.333333 h; Microwave irradiation;
参考文献
Al-Masum, Mohammad; Welch, Rebecca L.
Tetrahedron Letters, 2014 , vol. 55, # 10 p. 1726 - 1728
反应条件
1: 5-tert-butyl-2'-(trifluoromethoxy)biphenylyl-2-diazonium hexafluoroantimonate in dichloromethane T=-100 - -90°C; 1.16667 h; Irradiation; 2: 4-nitro-phenol With N-ethyl-N,N-diisopropylamine in dichloromethane T=-90 - -10°C; 3 h; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 72, # 18 p. 6905 - 6917
反应条件
nitronium tetrafluoroborate in nitromethane T=25°C; 2 h; further nitrating reagents, solvents and temperature; investigation of the nitration reaction; Hammett-Brown plot (relative reactivity data compared to benzene); Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 109, p. 3708
反应条件
hydrogen; ShPAK-0.5 in methanol T=44 - 46°C; P=29420.3 - 30891.3 Torr;
参考文献
Kislyi; Tolkacheva; Semenov
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 2 p. 269 - 271
参考文献
McEvoy,F.J. et al.
Journal of Medicinal Chemistry, 1968 , vol. 11, # 6 p. 1248 - 1250