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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
9-氨基-2-羟基吖啶
合成路线
（共 13 条）
3407-99-6
2-甲氧基吖啶-9-胺
→
反应条件
7132-67-4
9-氨基-2-羟基吖啶
反应条件
water; hydrogen bromide 3 h; Heating;
参考文献
Tomosaka, Hideyuki; Anzai, Kentaro; Hasegawa, Eietsu; Horigome, Tsuneyoshi; Omata, Saburo
Bioscience, Biotechnology and Biochemistry, 1996 , vol. 60, # 4 p. 714 - 716
202657-84-9
→
反应条件
7132-67-4
9-氨基-2-羟基吖啶
反应条件
potassium hydroxide 1 h; Heating;
参考文献
Del Giudice, Maria Rosaria; Borioni, Anna; Mustazza, Carlo; Gatta, Franco
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 6 p. 1661 - 1667
4746-97-8
1,4-环己二酮单乙二醇缩酮
→
反应条件
7132-67-4
9-氨基-2-羟基吖啶
反应条件
1: 62 percent / NH3 (gas) / ethane-1,2-diol / 1 h / 150 - 160 °C 2: 87 percent / 30percent aq. H2O2 / acetic acid / 5 h / 80 °C 3: 78 percent / 1 h / 90 °C 4: 69 percent / Br2, MeOH / 0.33 h / Heating 5: 92 percent / 10percent aq. HCl / 1 h / 40 °C 6: 54 percent / 20percent aq. KOH / 1 h / Heating View Scheme
参考文献
Del Giudice, Maria Rosaria; Borioni, Anna; Mustazza, Carlo; Gatta, Franco
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 6 p. 1661 - 1667
91-56-5
吲哚-2,3-二酮
→
反应条件
7132-67-4
9-氨基-2-羟基吖啶
反应条件
1: 62 percent / NH3 (gas) / ethane-1,2-diol / 1 h / 150 - 160 °C 2: 87 percent / 30percent aq. H2O2 / acetic acid / 5 h / 80 °C 3: 78 percent / 1 h / 90 °C 4: 69 percent / Br2, MeOH / 0.33 h / Heating 5: 92 percent / 10percent aq. HCl / 1 h / 40 °C 6: 54 percent / 20percent aq. KOH / 1 h / Heating View Scheme
参考文献
Del Giudice, Maria Rosaria; Borioni, Anna; Mustazza, Carlo; Gatta, Franco
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 6 p. 1661 - 1667
104-92-7
4-溴苯甲醚
→
反应条件
7132-67-4
9-氨基-2-羟基吖啶
反应条件
1: 27 percent / Na2CO3, Cu / butan-1-ol / 24 h / Heating 2: POCl3 / 2 h / Heating 3: 0.08 h / 70 °C 4: 1.03 g / (NH4)2CO3, phenol / 0.75 h / 120 °C 5: 86.9 percent / HBr, H2O / 3 h / Heating View Scheme
参考文献
Tomosaka, Hideyuki; Anzai, Kentaro; Hasegawa, Eietsu; Horigome, Tsuneyoshi; Omata, Saburo
Bioscience, Biotechnology and Biochemistry, 1996 , vol. 60, # 4 p. 714 - 716
118-92-3
邻氨基苯甲酸
→
反应条件
7132-67-4
9-氨基-2-羟基吖啶
反应条件
1: 27 percent / Na2CO3, Cu / butan-1-ol / 24 h / Heating 2: POCl3 / 2 h / Heating 3: 0.08 h / 70 °C 4: 1.03 g / (NH4)2CO3, phenol / 0.75 h / 120 °C 5: 86.9 percent / HBr, H2O / 3 h / Heating View Scheme
参考文献
Tomosaka, Hideyuki; Anzai, Kentaro; Hasegawa, Eietsu; Horigome, Tsuneyoshi; Omata, Saburo
Bioscience, Biotechnology and Biochemistry, 1996 , vol. 60, # 4 p. 714 - 716
16492-13-0
9-氯-2-甲氧基吖啶
→
反应条件
7132-67-4
9-氨基-2-羟基吖啶
反应条件
1: 0.08 h / 70 °C 2: 1.03 g / (NH4)2CO3, phenol / 0.75 h / 120 °C 3: 86.9 percent / HBr, H2O / 3 h / Heating View Scheme
参考文献
Tomosaka, Hideyuki; Anzai, Kentaro; Hasegawa, Eietsu; Horigome, Tsuneyoshi; Omata, Saburo
Bioscience, Biotechnology and Biochemistry, 1996 , vol. 60, # 4 p. 714 - 716
110166-26-2
→
反应条件
7132-67-4
9-氨基-2-羟基吖啶
反应条件
Salmonella typhimurium TA 1537
参考文献
Tomosaka, Hideyuki; Anzai, Kentaro; Hasegawa, Eietsu; Horigome, Tsuneyoshi; Omata, Saburo
Bioscience, Biotechnology and Biochemistry, 1996 , vol. 60, # 4 p. 714 - 716
202657-71-4
→
反应条件
7132-67-4
9-氨基-2-羟基吖啶
反应条件
1: 78 percent / 1 h / 90 °C 2: 69 percent / Br2, MeOH / 0.33 h / Heating 3: 92 percent / 10percent aq. HCl / 1 h / 40 °C 4: 54 percent / 20percent aq. KOH / 1 h / Heating View Scheme
参考文献
Del Giudice, Maria Rosaria; Borioni, Anna; Mustazza, Carlo; Gatta, Franco
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 6 p. 1661 - 1667
202657-78-1
→
反应条件
7132-67-4
9-氨基-2-羟基吖啶
反应条件
1: 92 percent / 10percent aq. HCl / 1 h / 40 °C 2: 54 percent / 20percent aq. KOH / 1 h / Heating View Scheme
参考文献
Del Giudice, Maria Rosaria; Borioni, Anna; Mustazza, Carlo; Gatta, Franco
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 6 p. 1661 - 1667
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