Lepiochlorin合成路线 （共 12 条）
反应条件
silver(I) acetate; acetic acid in tetrahydrofuran; water
参考文献
Donaubauer, John R.; McMorris, Trevor C.
Tetrahedron Letters, 1980 , vol. 21, p. 2771 - 2772
反应条件
quinoline; hydrogen; Pd-BaSO4 in ethanol
参考文献
Caine, Drury; Ukachukwu, Victoria C.
Tetrahedron Letters, 1983 , vol. 24, # 37 p. 3959 - 3960
反应条件
hydrogenchloride in 1,4-dioxane
6 h; Heating;
参考文献
Torii; Inokuchi; Kondo
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 7 p. 2183 - 2184
反应条件
1: N-bromosuccinimide, benzoylperoxide / CCl4 / 26 h / Heating
2: 65 percent / silver acetate / acetic acid / tetrahydrofuran; H2O
View Scheme
参考文献
Donaubauer, John R.; McMorris, Trevor C.
Tetrahedron Letters, 1980 , vol. 21, p. 2771 - 2772
反应条件
1: 80 percent / thionyl chloride, pyridine / CHCl3 / Heating
2: N-bromosuccinimide, benzoylperoxide / CCl4 / 26 h / Heating
3: 65 percent / silver acetate / acetic acid / tetrahydrofuran; H2O
View Scheme
参考文献
Donaubauer, John R.; McMorris, Trevor C.
Tetrahedron Letters, 1980 , vol. 21, p. 2771 - 2772
反应条件
1: 85 percent / 3N hydrochloric acid / diethyl ether / 4.5 h / Heating
2: 80 percent / thionyl chloride, pyridine / CHCl3 / Heating
3: N-bromosuccinimide, benzoylperoxide / CCl4 / 26 h / Heating
4: 65 percent / silver acetate / acetic acid / tetrahydrofuran; H2O
View Scheme
参考文献
Donaubauer, John R.; McMorris, Trevor C.
Tetrahedron Letters, 1980 , vol. 21, p. 2771 - 2772
反应条件
1: m-chloroperbenzoic acid
2: benzene / Heating
3: 85 percent / 3N hydrochloric acid / diethyl ether / 4.5 h / Heating
4: 80 percent / thionyl chloride, pyridine / CHCl3 / Heating
5: N-bromosuccinimide, benzoylperoxide / CCl4 / 26 h / Heating
6: 65 percent / silver acetate / acetic acid / tetrahydrofuran; H2O
View Scheme
参考文献
Donaubauer, John R.; McMorris, Trevor C.
Tetrahedron Letters, 1980 , vol. 21, p. 2771 - 2772
反应条件
1: benzene / Heating
2: 85 percent / 3N hydrochloric acid / diethyl ether / 4.5 h / Heating
3: 80 percent / thionyl chloride, pyridine / CHCl3 / Heating
4: N-bromosuccinimide, benzoylperoxide / CCl4 / 26 h / Heating
5: 65 percent / silver acetate / acetic acid / tetrahydrofuran; H2O
View Scheme
参考文献
Donaubauer, John R.; McMorris, Trevor C.
Tetrahedron Letters, 1980 , vol. 21, p. 2771 - 2772
反应条件
in diethyl ether
T=-78°C; 3 h;
参考文献
Caine, Drury; Ukachukwu, Victoria C.
Tetrahedron Letters, 1983 , vol. 24, # 37 p. 3959 - 3960
反应条件
1: 88 percent / NH4Cl / electrochemical halogenation
2: 86 percent / aq. HCl / dioxane / 6 h / Heating
View Scheme
参考文献
Torii; Inokuchi; Kondo
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 7 p. 2183 - 2184
