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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
7135-32-2
合成路线
（共 46 条）
7135-32-2
→
反应条件
100510-99-4
反应条件
1: conc. aq. NaOH, N-benzyltributylammonium bromide / 3 h / 60 °C 2: Na, NH3 3: 80percent aq. H2SO4, conc. aq. HNO3 (d = 1.5) / 0.5 h 4: H2 / 10percent Pd/C / ethanol View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 30, # 8 p. 1279 - 1287
591-50-4
碘苯
+
7135-32-2
→
反应条件
3335-95-3
反应条件
1: With tBu3PHBF4; bis(dibenzylideneacetone)-palladium(0) in toluene Inert atmosphere; 2: With lithium hexamethyldisilazane in toluene T=20°C; 5 h;
参考文献
Mai, Cheng-Kang; Sammons, Matthew F.; Sammakia, Tarek
Organic Letters, 2010 , vol. 12, # 10 p. 2306 - 2309
108-86-1
溴代苯
+
7135-32-2
→
反应条件
3335-95-3
反应条件
potassium hexamethylsilazane; bis(dibenzylideneacetone)-palladium(0); 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran; toluene T=70°C; 0.5 h; Inert atmosphereSealed tube;
参考文献
Durbin, Matthew J.; Willis, Michael C.
Organic Letters, 2008 , vol. 10, # 7 p. 1413 - 1415
7135-32-2
+
17763-67-6
苯基三氟甲烷磺酸酯
→
反应条件
3335-95-3
反应条件
potassium hexamethylsilazane; bis(dibenzylideneacetone)-palladium(0); 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran; toluene T=70°C; 0.5 h; Inert atmosphereSealed tube;
参考文献
Durbin, Matthew J.; Willis, Michael C.
Organic Letters, 2008 , vol. 10, # 7 p. 1413 - 1415
7135-32-2
+
108-90-7
氯苯
→
反应条件
3335-95-3
反应条件
potassium hexamethylsilazane; bis(dibenzylideneacetone)-palladium(0); 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran; toluene T=70°C; 0.5 h; Inert atmosphereSealed tube;
参考文献
Durbin, Matthew J.; Willis, Michael C.
Organic Letters, 2008 , vol. 10, # 7 p. 1413 - 1415
1217-89-6
1-苄基-1H-吲哚-2,3-二酮
→
反应条件
7135-32-2
反应条件
NH2NH2•xH2O T=130°C; Wolff-Kishner reduction; 3 h; Inert atmosphere;
参考文献
Horne, David A.; Jove, Richard; Lincoln, Christopher; Nam, Sangkil; Overman, Larry; Xie, Jun
Patent: US2013/225637 A1, 2013 ;
Location in patent: Paragraph 0138-0139 ;
178809-24-0
→
反应条件
7135-32-2
反应条件
[2-(8-methoxynaphthalen-1-yl)phenyl]diphenylphosphane; caesium carbonate; palladium diacetate in 1,4-dioxane T=100°C; 3.5 h;
参考文献
Kitamura, Yuki; Hashimoto, Ayano; Yoshikawa, Seiji; Odaira, Jun-Ichi; Furuta, Takumi; Kan, Toshiyuki; Tanaka, Kiyoshi
Synlett, 2006 , # 1 art. no. U28205ST, p. 115 - 117
2444-36-2
邻氯苯乙酸
+
100-46-9
苄胺
→
反应条件
7135-32-2
反应条件
1: T=150°C; 0.5 h; microwave irradiation; 2: With sodium hydroxide; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; palladium diacetate in water; toluene T=100°C; 0.5 h; microwave irradiation;
参考文献
Poondra, Rajamohan R.; Turner, Nicholas J.
Organic Letters, 2005 , vol. 7, # 5 p. 863 - 866
18698-97-0
邻溴苯乙酸
+
100-46-9
苄胺
→
反应条件
7135-32-2
反应条件
1: T=150°C; 0.5 h; microwave irradiation; 2: With sodium hydroxide; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; palladium diacetate in water; toluene T=100°C; 0.5 h; microwave irradiation;
参考文献
Poondra, Rajamohan R.; Turner, Nicholas J.
Organic Letters, 2005 , vol. 7, # 5 p. 863 - 866
74585-36-7
→
反应条件
7135-32-2
+
343221-51-2
反应条件
KNH2 in ammonia; benzene 0.5 h; Irradiation;
参考文献
Goehring, R. Richard; Sachdeva, Yesh P.; Pisipati, Jyothi S.; Sleevi, Mark C.; Wolfe, James F.
Journal of the American Chemical Society, 1985 , vol. 107, # 2 p. 435 - 443
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