(E)-12-十四碳烯-9-炔-1-醇乙酸酯合成路线 （共 6 条）
反应条件
hydrogen; sodium tetrahydroborate; nickel diacetate; ethylenediamine in ethanol Ambient temperature;
参考文献
Odinokov, V. N.; Dzhemilev, U. M.; Ishumuratov, G. Yu.; Botsman, L. P.; Ibragimov, A. G.; et al.
Chemistry of Natural Compounds, 1991 , vol. 27, # 2 p. 238 - 240
Khimiya Prirodnykh Soedinenii, 1991 , # 2 p. 276 - 279
反应条件
1: 1.) EtMgBr, 2.) CuBr / 1.) THF, heating, 1 h, 2.) reflux, 1 h, then at r. t., 36 h
2: acetic acid / 12 h / 80 °C
View Scheme
参考文献
Rossi, Renzo; Carpita, Adriano; Gaudenzi, Loretta; Quirici, Maria Grazia
Gazzetta Chimica Italiana, 1980 , vol. 110, # 4 p. 237 - 246
反应条件
in acetic acid
T=80°C; 12 h; Yield given;
参考文献
Rossi, Renzo; Carpita, Adriano; Gaudenzi, Loretta; Quirici, Maria Grazia
Gazzetta Chimica Italiana, 1980 , vol. 110, # 4 p. 237 - 246
反应条件
pyridine; lithium amide
Yield given. Multistep reaction;
参考文献
Kasymzhanova, M.; Abdukakharov, V. S.; Abduvakhabov, A. A.
Chemistry of Natural Compounds, 1992 , vol. 28, # 5 p. 525 - 526
Khimiya Prirodnykh Soedinenii, 1992 , # 5 p. 598 - 599
反应条件
Yield given. Multistep reaction;
参考文献
Kasymzhanova, M.; Abdukakharov, V. S.; Kamaev, F. G.; Abduvakhabov, A. A.
Chemistry of Natural Compounds, 1989 , vol. 25, # 6 p. 708 - 713
Khimiya Prirodnykh Soedinenii, 1989 , # 6 p. 834 - 840
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Odinokov, V. N.; Dzhemilev, U. M.; Ishumuratov, G. Yu.; Botsman, L. P.; Ibragimov, A. G.; et al.
Chemistry of Natural Compounds, 1991 , vol. 27, # 2 p. 238 - 240
Khimiya Prirodnykh Soedinenii, 1991 , # 2 p. 276 - 279
