反应条件
1: 71 percent / BuLi / tetrahydrofuran / 1.) 0 deg C, 30 min, 2.) -78 deg C, 2 h
2: 91 percent / LiAlH4 / diethyl ether / 2.5 h / 0 °C
3: 1.) MCPBA / 1.) CHCl3, 0 deg C, 30 min, 2.) r.t., 48 h
4: 94 percent / Na, NH3 / tetrahydrofuran / 1.5 h / -78 °C
5: 70 percent / H2 / 5percent Rh/Al2O3 / ethanol / 18 h / 20 °C / 3800 Torr
View Scheme
参考文献
Davies, Stephen G.; Smyth, G. Darren
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 20 p. 2467 - 2477
