N3P3Cl4(NH2)2 in diethyl ether
17 h; Ambient temperatureexcess dimethylamine;
参考文献
Lensink, Cees; Ruiter, Barteld de; Grampel, Johan C. van de
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 1521 - 1526
in acetonitrile
byproducts: NH2(CH3)2Cl; addn. of excess of NH(CH3)2 at -78°C for 2 h, then 8 h reflux; crystd. from light petroleum; elem. anal.;
参考文献
Kilic, Zeynel; Guenduez, Necla; Kilic, Emine; Nazir, Hasan
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1989 , vol. 19, p. 453 - 468
in diethyl ether
byproducts: NH2(CH3)2Cl; addn. of excess of NH(CH3)2 at -78°C for 2 h, then 8 h reflux; crystn.; elem. anal.;
参考文献
Kilic, Zeynel; Guenduez, Necla; Kilic, Emine; Nazir, Hasan
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1989 , vol. 19, p. 453 - 468
