二苯基[4-(苯基硫代)苯基]-六氟锑酸锍合成路线 (共 3 条)
反应条件
potassium hexafluoroantimonate; sulfuric acid; acetic anhydride in acetonitrile T=45°C; 1 h; Product distribution / selectivity;
参考文献
San-Apro Limited
Patent: EP1350789 A1, 2003 ;
Location in patent: Page/Page column 7-8 ;
反应条件
1: With potassium hexafluoroantimonate; sulfuric acid; acetic acid in water 0.5 h; 2: 4,4'-diphenylsulfide; bis-(phenyl)-sulfoxide With acetic anhydride in water T=20 - 75°C; 1.5 h; Product distribution / selectivity;
参考文献
EP1640363 A1, ;
Page/Page column 11 ;
反应条件
copper acetylacetonate in chlorobenzene 3 h; Heating;
参考文献
Journal of the American Chemical Society, , vol. 112, # 16 p. 6004 - 6015