2,3-二甲基-2-己烯合成路线 （共 16 条）
反应条件
platinum on activated charcoal T=160 - 170°C; Hydrogenation;
参考文献
Lewina et al.
Doklady Akademii Nauk SSSR, 1950 , vol. 75, p. 39,41
Chem.Abstr., 1951 , p. 4637
反应条件
1percent Pt, 0.4percent K, 2.4percent Sn, 5percent La and 91.2percent La-Ce-ZrO2 support; activated with H2 at 400 deg C T=525°C; P=2250.23 Torr; 1 h; tubular reactor; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2009/326287 A1, 2009 ;
Location in patent: Page/Page column 14 ;
反应条件
phosphoric acid pumice stone
T=250°C;
参考文献
Boord et al.
Industrial and Engineering Chemistry, 1949 , vol. 41, p. 615
Show Details
Henne; Matuszak
Journal of the American Chemical Society, 1944 , vol. 66, p. 1651
参考文献
Clennan, Edward L.; Chen, Xiangning; Koola, Jaya J.
Journal of the American Chemical Society, 1990 , vol. 112, # 13 p. 5193 - 5199
反应条件
titanium oxide support DT51 compacted with H2O and formic acid; calcined at 500 deg C; activated at 200 deg C in N2 stream
T=25°C; P=15001.5 Torr; tubular reactor; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2009/326287 A1, 2009 ;
Location in patent: Page/Page column 13 ;
参考文献
Whitmore; Evers
Journal of the American Chemical Society, 1933 , vol. 55, p. 813
反应条件
pyridine; thionyl chloride
参考文献
Lomas,J.S. et al.
Tetrahedron Letters, 1971 , p. 599 - 602
反应条件
hydrogenchloride
T=-20 - -15°C; und Behandeln des Reaktionsprodukts mit Aethylmagnesiumbromid in Aether bei -30grad bis -20grad;
参考文献
Lewina et al.
Doklady Akademii Nauk SSSR, 1950 , vol. 75, p. 39,41
Chem.Abstr., 1951 , p. 4637
反应条件
T=350 - 400°C; Produkt 5: 2.3-Dimethyl-hexen-(3);
参考文献
Boord et al.
Industrial and Engineering Chemistry, 1949 , vol. 41, p. 615
Show Details
Henne; Matuszak
Journal of the American Chemical Society, 1944 , vol. 66, p. 1651
反应条件
1: phosphoric acid
2: 420 - 430 °C
3: hydrogen chloride / -20 - -15 °C / und Behandeln des Reaktionsprodukts mit Aethylmagnesiumbromid in Aether bei -30grad bis -20grad
View Scheme
参考文献
Lewina et al.
Doklady Akademii Nauk SSSR, 1950 , vol. 75, p. 39,41
Chem.Abstr., 1951 , p. 4637
