3-氯-6-甲基磺酰基吡嗪合成路线 （共 5 条）
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=0°C; 0.5 h; Inert atmosphere;
参考文献
Daiichi Sankyo Company, Limited
Patent: EP2239253 A1, 2010 ;
Location in patent: Page/Page column 156 ;
EP 2239253 A1
反应条件
sodium methylate in methanol
T=60°C; 0.5 h; Inert atmosphere;
参考文献
Daiichi Sankyo Company, Limited
Patent: EP2239253 A1, 2010 ;
Location in patent: Page/Page column 156 ;
EP 2239253 A1
反应条件
in N,N-dimethyl-formamide
T=20°C;
参考文献
MERCK andamp; CO., INC.; CHOBANIAN, Harry; LIN, Linus, S.; LIU, Ping; CHIODA, Marc, D.; DEVITA, Robert, J.; NARGUND, Ravi, P.; GUO, Yan
Patent: WO2010/17079 A1, 2010 ;
Location in patent: Page/Page column 90 ;
WO 2010/017079 A1
反应条件
[MoCl5]; zinc in tetrahydrofuran; water
0.75 h; Heating;
参考文献
Polanc, Slovenko; Stanovnik, Branko; Tisler, Miha
Synthesis, 1980 , # 2 p. 129 - 131
反应条件
in toluene
1 h; Heating;
参考文献
Stanovnik, Branko; Tisler, Miha; Hribar, Alenka; Barlin, Gordon B.; Brown, Desmond J.
Australian Journal of Chemistry, 1981 , vol. 34, # 8 p. 1729 - 1738
