反式-1-(溴甲基)-4-丙基环己烷合成路线 （共 6 条）
反应条件
sulfuric acid; hydrogen bromide
参考文献
Carr; Gray; McDonnell
Molecular crystals and liquid crystals, 1982 , vol. 97, # 1-4 p. 13 - 28
反应条件
1: 100 percent / SOCl2 2: 91 percent / LiAlH4 / diethyl ether 3: 76 percent / HBr, aq/H2SO4 View Scheme
参考文献
Molecular crystals and liquid crystals, , vol. 97, # 1-4 p. 13 - 28
反应条件
1: 91 percent / LiAlH4 / diethyl ether 2: 76 percent / HBr, aq/H2SO4 View Scheme
参考文献
Molecular crystals and liquid crystals, , vol. 97, # 1-4 p. 13 - 28
反应条件
1: trans-4-lt;trans-4-Pentylcyclohexylgt;cyclohexanol With sodium hydride in tetrahydrofuran 2: trans-4-n-propyl-1-bromomethylcyclohexane in tetrahydrofuran 2 h; Heating / reflux;
参考文献
CLARIANT INTERNATIONAL LTD.
Patent: EP1518851 A1, 2005 ;
Location in patent: Page/Page column 9-11 ;
反应条件
1: trans-4-n-propylcyclohexanol With sodium hydride in tetrahydrofuran 2: trans-4-n-propyl-1-bromomethylcyclohexane in tetrahydrofuran 2 h; Heating / reflux;
参考文献
CLARIANT INTERNATIONAL LTD.
Patent: EP1518851 A1, 2005 ;
Location in patent: Page/Page column 10; 11 ;
反应条件
1: 93 percent / dimethylsulfoxide
2: 78 percent / H2SO4 / acetic acid
View Scheme
参考文献
Takatsu; Takeuchi; Sato
Molecular crystals and liquid crystals, 1983 , vol. 100, # 3-4 p. 345 - 355
