1: NaHCO3 / ethanol / 48 h / Ambient temperature 2: 1.) Mg / 1.) THF, reflux, 2.) THF, r.t., 48 h 3: 74 percent / t-BuOK / tetrahydrofuran / 0.5 h / 0 °C View Scheme
参考文献
Bull, Steven D.; Davies, Stephen G.; Jones, Simon; Sanganee, Hitesh J.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 4 p. 387 - 398
1: NaHCO3 / ethanol / 48 h / Ambient temperature 2: 1.) Mg / 1.) Et2O, reflux, 2.) Et2O, r.t., 48 h 3: 72 percent / t-BuOK / tetrahydrofuran / 0.5 h / 0 °C View Scheme
参考文献
Bull, Steven D.; Davies, Stephen G.; Jones, Simon; Sanganee, Hitesh J.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 4 p. 387 - 398
