4-氯-5-甲基-2-硝基苯酚合成路线 (共 19 条)
反应条件
Al(NO3)3*9H2O; sulfuric acid; silica gel; silica gel in dichloromethane T=20°C; 1.83333 h;
参考文献
Ghorbani-Choghamarani, Arash; Goudarziafshar, Hamid; Nikoorazm, Mohsen; Yousefi, Somaieh
Canadian Journal of Chemistry, 2009 , vol. 87, # 8 p. 1144 - 1147
反应条件
acetic acid; sodium nitrite T=14 - 18°C;
参考文献
Journal of the American Chemical Society, , vol. 55, p. 2125,2129
反应条件
nitric acid in acetic anhydride T=-60°C; Yields of byproduct given;
参考文献
Tetrahedron, , vol. 45, # 5 p. 1299 - 1310
反应条件
nitric acid; trifluoroacetic anhydride in chloroform T=-40°C;
参考文献
Tetrahedron, , vol. 45, # 5 p. 1299 - 1310
反应条件
[EtNH3][NO3]; trifluoroacetic anhydride T=-5 - 0°C; 0.166667 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 76, # 19 p. 8088 - 8094
反应条件
nitric acid in acetic anhydride 1.) -60 deg C; 2.) 0 deg C;
参考文献
Tetrahedron, , vol. 45, # 5 p. 1299 - 1310
反应条件
nitric acid in chloroform 1.) -60 deg C; 2.) rt; Yield given;
参考文献
Tetrahedron, , vol. 45, # 5 p. 1299 - 1310
反应条件
chlorine; acetic acid
参考文献
Journal of the Chemical Society, , vol. 105, p. 1891
反应条件
nitric acid; acetic acid
参考文献
Journal of the Chemical Society, , vol. 105, p. 1891
反应条件
sulfuryl dichloride; 2,2'-azo-bisisobutyronitrile 3 h; Heating;
参考文献
Russian Journal of Organic Chemistry, , vol. 32, # 3 p. 394 - 400