1-(1-吡咯烷)环戊烯合成路线 （共 78 条）
反应条件
Yield given. Multistep reaction;
参考文献
Fisher, Gary B.; Goralski, Christian T.; Nicholson, Lawrence W.; Hasha, Dennis L.; Zakett, Donald; Singaram, Bakthan
Journal of Organic Chemistry, 1995 , vol. 60, # 7 p. 2026 - 2034
反应条件
1: (i) , (ii) aq. HCl 2: <PhCH2NMe3>OH / methanol 3: aq. HCl / acetic acid / Heating View Scheme
参考文献
Fusco,R. et al.
Farmaco, Edizione Scientifica, 1965 , vol. 20, p. 393 - 407
反应条件
acetic acid 1) THF, reflux, overnight 2) 100 deg C, 4 h; Yield given. Multistep reaction;
参考文献
Rodriguez, Jose-Gonzalo; Andres, Angel San
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 5 p. 1293 - 1299
反应条件
hydrogenchloride 1.) toluene, - 20 deg C, 48 h, 2.) acetone, 0 deg C; Yield given. Multistep reaction;
参考文献
Gazzetta Chimica Italiana, , vol. 115, # 12 p. 663 - 668
反应条件
2.) S 1.) xylene, reflux, 18 h; 2.) 220 deg C, 40 min; Yield given. Multistep reaction;
参考文献
Tang, Ping Wah; Maggiulli, Cataldo A.
Journal of Organic Chemistry, 1981 , vol. 46, # 17 p. 3429 - 3432
反应条件
in xylene 18 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tang, Ping Wah; Maggiulli, Cataldo A.
Journal of Organic Chemistry, 1981 , vol. 46, # 17 p. 3429 - 3432
反应条件
in 1,4-dioxane 12 h;
参考文献
El-Barbary, A. A.; Carlsson, S.; Lawesson, S.-O.
Tetrahedron, 1982 , vol. 38, # 3 p. 405 - 412
反应条件
1: 91 percent / diethyl ether / 2 h / Ambient temperature 2: 72 percent / 1 N HCl / diethyl ether / 4 h / 35 - 40 °C View Scheme
参考文献
Buttke; Niclas
Advanced Synthesis and Catalysis, 1996 , vol. 338, # 7 p. 681 - 683
反应条件
1,4-dioxane; triethylamine anschliessend Behandeln mit wss. HCl;
参考文献
Kuehne
Journal of the American Chemical Society, 1959 , vol. 81, p. 5400,5403
反应条件
1: (i) (heating in benzene), (ii) H2O
2: TsOH
View Scheme
参考文献
Meyers,A.I. et al.
Journal of Organic Chemistry, 1973 , vol. 38, p. 36 - 56
