2-乙酰氧基-3-甲氧基苯甲醛合成路线 （共 22 条）
反应条件
1: 1.) Br2, KBr, 2.) NaOH / 1.) H2O, 6 h, 2.) H2O, 6 h
2: 96 percent / K2CO3 / dimethylformamide / 5 h / 110 - 120 °C
3: 70 percent / KMnO4 / acetone; H2O / 3 h / 50 - 60 °C
4: 90.7 percent / SOCl2 / benzene / 1 h / Heating
View Scheme
参考文献
Nimgirawath, Surachai; Ponghusabun, Ong-ard
Australian Journal of Chemistry, 1994 , vol. 47, # 5 p. 951 - 956
反应条件
1: 99 percent / Br2, potassium bromide / H2O / 24 h / 25 °C
2: 95 percent / aq. NaOH / 4 h / 25 °C
3: 82 percent / aq. NaOH, H2O2 / 4 h / 25 °C
4: K2CO3, cupric oxide / 5.5 h / 110 °C
View Scheme
参考文献
Simig, Gy.; Schlosser, M.
ACH - Models in Chemistry, 1994 , vol. 131, # 2 p. 217 - 228
