3-甲氧基-4-甲基苯甲酸合成路线 (共 34 条)
反应条件
n-butyllithium; potassium tert-butylate in tetrahydrofuran; hexane T=-78°C; Alkylation; 1.66667 h;
参考文献
Sinha, Surajit; Mandal, Bhubaneswar; Chandrasekaran, Srinivasan
Tetrahedron Letters, 2000 , vol. 41, # 17 p. 3157 - 3160
反应条件
N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium in tetrahydrofuran; hexane; cyclohexane 1.) -90 deg C, 60 min, 2.) -78 deg C;
参考文献
Journal of Organic Chemistry, , vol. 59, # 15 p. 4042 - 4044
参考文献
Chemische Berichte, , vol. 11, p. 1587
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 42, # 7 p. 2240 - 2245
反应条件
diethyl ether; magnesium anschliessend mit CO2 behandeln;
参考文献
Journal of the Chemical Society, , p. 1285,1287
Acta Chemica Scandinavica (1947-1973), , vol. 6, p. 1137,1400
反应条件
1: aqueous NaOH 2: magnesium; diethyl ether / anschliessend mit CO2 behandeln View Scheme
参考文献
Journal of the Chemical Society, , p. 1285,1287
Acta Chemica Scandinavica (1947-1973), , vol. 6, p. 1137,1400
参考文献
Gazzetta Chimica Italiana, , vol. 10, p. 516
Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften, , p. 663
参考文献
Jahresbericht ueber die Fortschritte der Chemie und Verwandter Theile Anderer Wissenschaften, , p. 663
参考文献
ICI Americas Inc.
Patent: US5047402 A1, 1991 ;
反应条件
hydrogenchloride; sulfuric acid; potassium carbonate; dimethyl sulfate; sodium nitrite in methanol; water; acetone
参考文献
Otsuka Pharmaceutical Co., Ltd.
Patent: US5409928 A1, 1995 ;
US 5409928 A