1-氯-2-亚甲基环己烷合成路线 （共 26 条）
反应条件
T=150°C; during glc;
参考文献
Hegde, Shridhar G.; Vogel, Martin K.; Saddler, John; Hrinyo, Tanya; Rockwell, Ned; et al.
Tetrahedron Letters, 1980 , vol. 21, p. 441 - 444
反应条件
Ca(OCl)2 in dichloromethane; water
slowly addition of dry ice to the mixture; Yield given;
参考文献
Hegde, Shridhar G.; Vogel, Martin K.; Saddler, John; Hrinyo, Tanya; Rockwell, Ned; et al.
Tetrahedron Letters, 1980 , vol. 21, p. 441 - 444
反应条件
1: sodium hydrogencarbonate; tetrachloromethane; chlorine
2: potassium acetate
3: aq.-ethanolic KOH-solution
4: diethyl ether; thionyl chloride
View Scheme
参考文献
Arnold; Lee
Journal of the American Chemical Society, 1953 , vol. 75, p. 5396,5399
反应条件
thionyl chloride; diethyl ether
参考文献
Arnold; Lee
Journal of the American Chemical Society, 1953 , vol. 75, p. 5396,5399
反应条件
1: lithium; diethyl ether / anschliessendes Behandeln mit Formaldehyd
2: diethyl ether; thionyl chloride
View Scheme
参考文献
Arnold; Lee
Journal of the American Chemical Society, 1953 , vol. 75, p. 5396,5399
反应条件
1: potassium acetate
2: aq.-ethanolic KOH-solution
3: diethyl ether; thionyl chloride
View Scheme
参考文献
Arnold; Lee
Journal of the American Chemical Society, 1953 , vol. 75, p. 5396,5399
反应条件
1: aq.-ethanolic KOH-solution
2: diethyl ether; thionyl chloride
View Scheme
参考文献
Arnold; Lee
Journal of the American Chemical Society, 1953 , vol. 75, p. 5396,5399
反应条件
tert-butylhypochlorite; silica gel in dichloromethane
0.5 h; Ambient temperature;
参考文献
Courtneidge, John L.; Bush, Melanie; Loh, Lay-See
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 12 p. 1539 - 1548
反应条件
phosphorus pentachloride
T=100°C;
参考文献
Mousseron; Jullien; Winternitz
Bulletin de la Societe Chimique de France, 1948 , p. 878,885
Show Details
Mousseron; Winternitz; Jullien
Bulletin de la Societe Chimique de France, 1947 , p. 80
反应条件
1: HCl / diethyl ether / 2 h / 13 °C
2: POCl3, pyridine
View Scheme
参考文献
Vereshchagin, A. N.; Kovylyaeva, G. I.; Bakaleinik, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 1 p. 91 - 95
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 1 p. 101 - 105
