3-硫氰酸基戊烷-2,4-二酮合成路线 (共 3 条)
反应条件
1: Pb(II) thiocyanate With iodobenzene dichloride in dichloromethane
T=0°C; 0.333333 h;
2: acetylacetone in dichloromethane
T=0 - 20°C; Further stages.;
参考文献
Prakash; Kaur; Batra; Rani; Singh; Moriarty
Journal of Organic Chemistry, 2001 , vol. 66, # 6 p. 2019 - 2023
反应条件
12-molybdophosphoric acid HPMo; copper dichloride in 1,2-dichloro-ethane
T=20°C; 0.75 h;
参考文献
Chaskar, Atul C.; Yadav, Arun A.; Langi, Bhushan P.; Murugappan, Anita; Shah, Chetan
Synthetic Communications, 2010 , vol. 40, # 19 p. 2850 - 2856
参考文献
Atkins, Elaine F.; Dabbs, Steven; Guy, Robert G.; Mahomed, Akbar A.; Mountford, Philip
Tetrahedron, 1994 , vol. 50, # 24 p. 7253 - 7264