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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-溴苯甲酰氯
合成路线
(共 144 条)
→
反应条件
1985-32-6
反应条件
MnCl2∙4H2O in tetrahydrofuran T=-30°C; 1 h; Inert atmosphere;
参考文献
Zhang, Fengmin; Shi, Zhuangzhi; Chen, Feng; Yuan, Yu
Applied Organometallic Chemistry, 2010 , vol. 24, # 1 p. 57 - 63
14097-41-7
+
7154-66-7
2-溴苯甲酰氯
→
反应条件
37481-45-1
反应条件
暂无反应条件数据
参考文献
Marion Laboratories, Inc.
Patent: US4022900 A1, 1977 ;
7154-66-7
2-溴苯甲酰氯
→
反应条件
17182-60-4
反应条件
1: triethylamine / dichloromethane / 25 °C 2: tetrahydrofuran / 0.5 h / 0 °C 3: tetrahydrofuran; ethanol 4: sodium hydride / ethylene glycol dimethyl ether View Scheme
参考文献
Song, Yoon Ju; Choi, Jin Sun; Lee, Jae In
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 10 p. 3117 - 3120
7154-66-7
2-溴苯甲酰氯
→
反应条件
18600-62-9
2-[(2-溴苯甲酰基)氨基]苯甲酸
反应条件
1: pyridine 2: aq. NaOH View Scheme
参考文献
Shen, Zengming; Ni, Zhenjie; Mo, Song; Wang, Jing; Zhu, Yamin
Chemistry - A European Journal, 2012 , vol. 18, # 16 p. 4859 - 4865
7154-66-7
2-溴苯甲酰氯
+
1026582-21-7
→
反应条件
189081-52-5
反应条件
N,N-diethylaniline in benzene 1 h; Heating; Yield given;
参考文献
Ishibashi, Hiroyuki; Kawanami, Hirotaka; Ikeda, Masazumi
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 6 p. 817 - 821
7154-66-7
2-溴苯甲酰氯
→
反应条件
26477-10-1
反应条件
1.1: nBuLi / tetrahydrofuran; hexane / 0.5 h / -78 - 20 °C 1.2: 80 percent / tetrahydrofuran; hexane / 2.17 h / -78 - 20 °C 2.1: 62 percent / tBuLi / pentane; tetrahydrofuran / 0.5 h / -100 - 20 °C 3.1: 92 percent / triethylsilyl hydride; TFA / CH2Cl2 / 2 h / 20 °C View Scheme
参考文献
Moreau, Anne; Couture, Axel; Deniau, Eric; Grandclaudon, Pierre
European Journal of Organic Chemistry, 2005 , # 16 p. 3437 - 3442
7154-66-7
2-溴苯甲酰氯
→
反应条件
23023-35-0
3-苯基-1-氨基异喹啉
反应条件
1: 1 h / 0 - 20 °C 2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / N,N-dimethyl-formamide / 3 h / 120 °C / |Microwave irradiation; |Inert atmosphere 3: ammonium acetate; NaAuCl4*2H2O; silver hexafluoroantimonate / acetonitrile / 20 h / 85 °C View Scheme
参考文献
Long, Yuhua; She, Zhigang; Liu, Xiaochen; Chen, Yu
Journal of Organic Chemistry, 2013 , vol. 78, # 6 p. 2579 - 2588
7154-66-7
2-溴苯甲酰氯
→
反应条件
反应条件
1: 1 h / 0 - 20 °C 2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / N,N-dimethyl-formamide / 3 h / 120 °C / |Microwave irradiation; |Inert atmosphere 3: ammonium acetate; NaAuCl4*2H2O; silver hexafluoroantimonate / acetonitrile / 20 h / 85 °C View Scheme
参考文献
Long, Yuhua; She, Zhigang; Liu, Xiaochen; Chen, Yu
Journal of Organic Chemistry, 2013 , vol. 78, # 6 p. 2579 - 2588
7154-66-7
2-溴苯甲酰氯
→
反应条件
82071-21-4
+
23023-35-0
3-苯基-1-氨基异喹啉
反应条件
1: 1 h / 0 - 20 °C 2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / N,N-dimethyl-formamide / 3 h / 120 °C / |Microwave irradiation; |Inert atmosphere 3: ammonium acetate; NaAuCl4*2H2O; silver hexafluoroantimonate / acetonitrile / 20 h / 85 °C View Scheme
参考文献
Long, Yuhua; She, Zhigang; Liu, Xiaochen; Chen, Yu
Journal of Organic Chemistry, 2013 , vol. 78, # 6 p. 2579 - 2588
7154-66-7
2-溴苯甲酰氯
→
反应条件
246181-55-5
反应条件
1: triethylamine / dichloromethane / 25 °C 2: tetrahydrofuran / 0.5 h / 0 °C 3: tetrahydrofuran; ethanol 4: sodium hydride / ethylene glycol dimethyl ether View Scheme
参考文献
Song, Yoon Ju; Choi, Jin Sun; Lee, Jae In
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 10 p. 3117 - 3120
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