乙基(2,2-二乙氧基乙基)氨基甲酸酯合成路线 (共 3 条)
反应条件
1: chloroformic acid ethyl ester With 1-hydroxy-pyrrolidine-2,5-dione; N-ethyl-N,N-diisopropylamine in dichloromethane
T=0 - 20°C; 3 h; Inert atmosphere;
2: 2,2-diethoxy-ethanamine in acetonitrile
T=20°C; Cooling with ice;
参考文献
REVIVA PHARMACEUTICALS, INC.
Patent: US2012/172426 A1, 2012 ;
Location in patent: Page/Page column 30 ;
反应条件
1: aq. NaHSO3
2: ethanol
View Scheme
参考文献
Bal'on,Ya.G.; Paranyuk,V.E.
Journal of Organic Chemistry USSR (English Translation), 1979 , vol. 15, p. 1073 - 1077
Zhurnal Organicheskoi Khimii, 1979 , vol. 15, p. 1203 - 1207
参考文献
Bal'on,Ya.G.; Paranyuk,V.E.
Journal of Organic Chemistry USSR (English Translation), 1979 , vol. 15, p. 1073 - 1077
Zhurnal Organicheskoi Khimii, 1979 , vol. 15, p. 1203 - 1207