6-羟基-1,4-苯并二恶烷6-乙酸酯合成路线 (共 4 条)
反应条件
sodium hydroxide in methanol 3 h; Ambient temperature;
参考文献
Besson, Thierry; Ruiz, Nicolas; Coudert, Gerard; Guillaumet, Gerald
Tetrahedron, 1995 , vol. 51, # 11 p. 3197 - 3204
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
参考文献
Bourlot, Anne-Sophie; Sanchez, Isabel; Dureng, Georges; Guillaumet, Gerald; Massingham, Roy; Monteil, Andre; Winslow, Eileen; Pujol, M. Dolors; Merour, Jean-Yves
Journal of Medicinal Chemistry, 1998 , vol. 41, # 17 p. 3142 - 3158
反应条件
1: 1.) NaNO2, H2SO4 / 1.) H2O, 0 deg C, 2.) 80 deg C
2: 1.) NaOH / 1.) RT, 2 h, 2.) 1 h
View Scheme
参考文献
Guillaumet, Gerald; Hretani, Mohamed; Coudert, Gerard; Averbeck, Dietrich; Averbeck, Simone
European Journal of Medicinal Chemistry, 1990 , vol. 25, # 1 p. 45 - 51
反应条件
sulfuric acid; benzene
参考文献
Heertjes et al.
Journal of the Chemical Society, 1957 , p. 3445