2-(2-吡啶)苯并噻唑合成路线 （共 40 条）
反应条件
[RuCl(CO)(PPh3)(PNS-Me)]; potassium hydroxide in toluene
T=100°C; 24 h;
参考文献
Ramachandran, Rangasamy; Prakash, Govindan; Selvamurugan, Sellappan; Viswanathamurthi, Periasamy; Malecki, Jan Grzegorz; Ramkumar, Venkatachalam
Dalton Transactions, 2014 , vol. 43, # 21 p. 7889 - 7902
反应条件
sodium acetate in methanol
T=15 - 20°C; Electrochemical reaction;
参考文献
Okimoto, Mitsuhiro; Yoshida, Takashi; Hoshi, Masayuki; Hattori, Kazuyuki; Komata, Masashi; Tomozawa, Kenta; Chiba, Tomohito
Heterocycles, 2008 , vol. 75, # 1 p. 35 - 42
反应条件
iron sulphate heptahydrate; oxygen in diethylene glycol dimethyl ether; water
T=150°C; 20 h; Sealed tube;
参考文献
Liu, Saiwen; Chen, Ru; Guo, Xiangyu; Yang, Huiqiong; Deng, Guojun; Li, Chao-Jun
Green Chemistry, 2012 , vol. 14, # 6 p. 1577 - 1580
反应条件
1: 2-amino-benzenethiol With trimethylaluminum chloride in toluene
T=0 - 20°C;
2: hydroxymethyl JandaJelTM resin-bound 2-pyridyl ester in toluene
24 h; Heating; Further stages.;
参考文献
Matsushita, Hana; Lee, Sang-Hyeup; Joung, Meyoungju; Clapham, Bruce; Janda, Kim D.
Tetrahedron Letters, 2004 , vol. 45, # 2 p. 313 - 316
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; copper(l) iodide in N,N-dimethyl-formamide
T=100°C; Suzuki-Miyaura cross-coupling reaction;
参考文献
Jones, Nicholas A.; Antoon, James W.; Bowie Jr., Alfred L.; Borak, J. Brian; Stevens, Erland P.
Journal of Heterocyclic Chemistry, 2007 , vol. 44, # 2 p. 363 - 367
反应条件
copper(l) iodide; 1,10-phenanthroline; Na2S*9H2O in acetic acid
T=100°C; 12 h; Sealed tube;
参考文献
Liu, Jidan; Gui, Qingwen; Yang, Zhiyong; Tan, Ze; Guo, Ruqing; Shi, Ji-Cheng
Synthesis (Germany), 2013 , vol. 45, # 7 art. no. SS-2012-F0968-OP, p. 943 - 951
反应条件
iodine in acetonitrile
T=20°C; 0.5 h;
参考文献
Naresh, Gunaganti; Kant, Ruchir; Narender, Tadigoppula
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 3821 - 3829
反应条件
Iron (III) nitrate nonahydrate; oxygen; [(t-Bu)3PH]BF4 in water; dimethyl sulfoxide
T=120°C; 24 h; Sealed tubeGreen chemistry;
参考文献
Khemnar, Ashok B.; Bhanage, Bhalchandra M.
RSC Advances, 2014 , vol. 4, # 18 p. 8939 - 8942
反应条件
air in chloroform
T=20°C; 5 h;
参考文献
Carlson, Lauren J.; Welby, Jenna; Zebrowski, Kelly A.; Wilk, Matthew M.; Giroux, Rachel; Ciancio, Nicole; Tanski, Joseph M.; Bradley, Amy; Tyler, Laurie A.
Inorganica Chimica Acta, 2011 , vol. 365, # 1 p. 159 - 166
反应条件
phosphorus trichoride in dichloromethane
5 h; Reflux;
参考文献
Fu, Xiao-Pu; Xuan, Qing-Qing; Liu, Li; Wang, Dong; Chen, Yong-Jun; Li, Chao-Jun
Tetrahedron, 2013 , vol. 69, # 22 p. 4436 - 4444
