3-氯-2-甲基-1H-吲哚合成路线 (共 6 条)
反应条件
trichloroisocyanuric acid; diphenyl diselenide; magnesium oxide in ethyl acetate
T=20°C;
参考文献
Silveira, Claudio C.; Wolf, Lucas; Martins, Guilherme M.; Von Muehlen, Lisandro; Mendes, Samuel R.
Tetrahedron, 2012 , vol. 68, # 51 p. 10464 - 10469,6
反应条件
copper dichloride in acetonitrile
4 h; Ambient temperature;
参考文献
Balogh-Hergovich, Eva; Speier, Gabor
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 2305 - 2309
反应条件
sulfuryl dichloride; diethyl ether
T=0°C;
参考文献
Mazzara; Borgo
Gazzetta Chimica Italiana, 1905 , vol. 35 II, p. 102
反应条件
sodium hypochlorite; potassium carbonate
1.) n-hexane/H2O, RT, 5 h, 2.) methanol/n-hexane, RT, 5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rosa, Michael De; Carbognani, Lante; Febres, Ayheza
Journal of Organic Chemistry, 1981 , vol. 46, # 10 p. 2054 - 2059
反应条件
sodium hypochlorite; potassium carbonate
1.) n-hexane/H2O, RT, 5 h, 2.) RT, 5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rosa, Michael De; Carbognani, Lante; Febres, Ayheza
Journal of Organic Chemistry, 1981 , vol. 46, # 10 p. 2054 - 2059
反应条件
sodium hydroxide; N-hexadecyl-N,N,N-trimethylammonium bromide in benzene
T=20°C; 24 h;
参考文献
Arumugam, Nagappan; Srinivasan, Panayencheri C.
Synthetic Communications, 2003 , vol. 33, # 13 p. 2313 - 2320