2-(二氟甲氧基)苯甲醛合成路线 （共 21 条）
反应条件
sodium hydroxide in 1,4-dioxane; hexane; 1-chloro-1,1-difluoro-methane; ethyl acetate
参考文献
US2002/35147 A1, ;
US 20020035147 A1
反应条件
sodium hydroxide; sodium dithionite in 1,4-dioxane; water T=65 - 70°C; 5 h;
参考文献
Shelyazhenko, S. V.; Fialkov, Yu. A.; Yagupol'skii, L. M.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 8.1 p. 1317 - 1324
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 8 p. 1652 - 1660
反应条件
potassium hydroxide in dichloromethane; water T=0°C; 0.5 h;
参考文献
Li, Lingchun; Wang, Fei; Ni, Chuanfa; Hu, Jinbo
Angewandte Chemie - International Edition, 2013 , vol. 52, # 47 p. 12390 - 12394
Angew. Chem., 2013 , vol. 125, # 47 p. 12616 - 12620,5
反应条件
hydrogenchloride in ethanol Heating;
参考文献
Kastron, V. V.; Vitolin', R. O.; Kanina, E. L.; Dubur, G. Ya.; Kimenis, A. A.
Pharmaceutical Chemistry Journal, 1987 , vol. 21, # 8 p. 571 - 574
Khimiko-Farmatsevticheskii Zhurnal, 1987 , vol. 21, # 8 p. 948 - 952
反应条件
hydrogenchloride in ethanol 8 h; Heating;
参考文献
Kastron, V. V.; Vitolin', R. O.; Kanina, E. L.; Dubur, G. Ya.; Kimenis, A. A.
Pharmaceutical Chemistry Journal, 1987 , vol. 21, # 8 p. 571 - 574
Khimiko-Farmatsevticheskii Zhurnal, 1987 , vol. 21, # 8 p. 948 - 952
反应条件
ammonium hydroxide in ethanol 12 h; Heating;
参考文献
Kastron, V. V.; Vitolin', R. O.; Dubur, G. Ya.; Skrastin'sh, I. P.; Kimenis, A. A.
Pharmaceutical Chemistry Journal, 1987 , vol. 21, # 5 p. 327 - 331
Khimiko-Farmatsevticheskii Zhurnal, 1987 , vol. 21, # 5 p. 554 - 559
反应条件
ammonium acetate in ethanol 4 h; Heating;
参考文献
Kolycheva, M. T.; Gerus, I. I.; Kukhar, V. P.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 11.2 p. 2134 - 2138
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 11 p. 2367 - 2372
反应条件
ammonium acetate in ethanol 4 h; Heating;
参考文献
Kolycheva, M. T.; Gerus, I. I.; Kukhar, V. P.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 11.2 p. 2134 - 2138
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 11 p. 2367 - 2372
反应条件
in acetic acid 2 h; Heating;
参考文献
Kastron, V. V.; Dubur, G. Ya.; Vitolin', R. O.; Skrastin'sh, I. P.; Kimenis, A. A.
Pharmaceutical Chemistry Journal, 1985 , vol. 19, # 5 p. 318 - 322
Khimiko-Farmatsevticheskii Zhurnal, 1985 , vol. 19, # 5 p. 545 - 549
反应条件
ammonium hydroxide in methanol 3 h; Heating;
参考文献
Kastron, V. V.; Dubur, G. Ya.; Vitolin', R. O.; Skrastin'sh, I. P.; Kimenis, A. A.
Pharmaceutical Chemistry Journal, 1985 , vol. 19, # 5 p. 318 - 322
Khimiko-Farmatsevticheskii Zhurnal, 1985 , vol. 19, # 5 p. 545 - 549
