1-(四氢-2H-吡喃-2-基氧基)十八碳-3,13-二炔合成路线 （共 4 条）
反应条件
1: 99 percent / PPTS / diethyl ether / 4 h / 60 °C 2: H2 / Pd/CaCO3 poisoned with Pb / hexane / 18 h 3: pyridine; DMAP View Scheme
参考文献
Abrams, Suzanne R.; Nucciarone, Donaato D.; Steck, Warren F.
Canadian Journal of Chemistry, 1983 , vol. 61, p. 1073 - 1076
反应条件
1: 99 percent / PPTS / diethyl ether / 4 h / 60 °C
2: LiAlH4 / 1,2-dimethoxy-ethane / 18 h / Heating
3: 91 percent / pyridine; DMAP
View Scheme
参考文献
Armstrong-Chong, Rosemary J.; Matthews, Kristopher; Chong, J. Michael
Tetrahedron, 2004 , vol. 60, # 45 p. 10239 - 10244
反应条件
1: 99 percent / PPTS / diethyl ether / 4 h / 60 °C
2: H2 / Pd/CaCO3 poisoned with Pb / hexane / 18 h
3: pyridine; DMAP
View Scheme
参考文献
Armstrong-Chong, Rosemary J.; Matthews, Kristopher; Chong, J. Michael
Tetrahedron, 2004 , vol. 60, # 45 p. 10239 - 10244
反应条件
1: 99 percent / PPTS / diethyl ether / 4 h / 60 °C
2: H2 / Pd/CaCO3 poisoned with Pb / hexane / 18 h
3: pyridine; DMAP
View Scheme
参考文献
Armstrong-Chong, Rosemary J.; Matthews, Kristopher; Chong, J. Michael
Tetrahedron, 2004 , vol. 60, # 45 p. 10239 - 10244
